| Код ТН ВЭД | 282200 |
Как аккредитованный DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure завод, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
| Упаковка | The DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure packaging consists of a 10 kg sealed plastic pail. |
| Погрузка контейнера (20-футовый контейнер) | Container Loading (20′ FCL): palletized chemical DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure, secured, ambient, with required transport documentation. |
| Доставка | DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure is typically shipped as a non-regulated, non-dangerous good. Use original, tightly sealed, light-blocking containers. Store cool, dry, away from heat, sparks, and direct sunlight. Always follow the current SDS and applicable local, national, and international transport regulations. |
| Хранение | Store in a cool, dry, well-ventilated area away from heat, sparks, open flames, and direct sunlight. Keep containers tightly closed in original packaging. Avoid freezing and temperatures above 30°C. Keep away from moisture. Segregate from oxidizers and incompatible materials. Use secondary containment, label clearly, and follow the manufacturer’s SDS and local regulations. Do not store near food, drink, or animal feed. |
| Срок годности | Shelf life is 12 months from manufacture when stored unopened in original container at 18–25°C, protected from sunlight and moisture. |
DSM Somos PerFORM Reflect is processed as a single-part photopolymer; no separate curative or diluent is added before stereolithography. Attempting solvent reduction changes the ceramic filler volume fraction and destabilizes postcure dimensional stability. In aerodynamic test model fabrication, the resin is built at 50 µm or 100 µm layer thickness on 355 nm solid-state laser systems with galvanometer scan heads. Resin bath temperature is held between 28 °C and 32 °C before each build to stabilize viscosity and filler suspension. The ceramic filler increases recoater blade contact friction relative to unfilled photopolymers. Blade condition is monitored through layer uniformity checks because a worn blade produces periodic thickness bands along the recoater travel direction. Before builds, the resin is recirculated with a low-shear impeller system operating below 60 rpm; direct high-shear mixing entrains air and increases microvoid content in vertical walls. Models with span dimensions beyond platform capability are sectioned along chord-wise and span-wise partition lines. Section joints are reinforced with machined aluminum alignment pins inserted into printed bushings and bonded with two-component epoxy film adhesive after thermal postcure. Sectional builds reduce accumulated shrinkage stress across the full span because individual sections are postcured before bonding. Support structures are generated with contact densities higher on leading-edge surfaces and lower on planar undersides. Layer contours are oriented so that curved leading edges are not parallel to the build direction. If leading edges are oriented parallel to the build direction, stair-step roughness amplifies boundary-layer effects and disturbs oil-flow visualization. As-built surfaces on 50 µm layers typically exhibit vertical-wall roughness between 0.4 µm and 1.2 µm Ra when measured according to ISO 4287. Wind-tunnel technicians apply a two-component epoxy primer and hand-sand leading edges to below 0.4 µm Ra before testing. Mechanical property acceptance data are generated according to ISO 527-2 for tensile modulus, ISO 178 for flexural strength, and ISO 75-2:2013 Method A for deflection temperature under load at 1.8 MPa. Thermal postcure is executed in a forced-air oven with a ramp rate not exceeding 0.5 °C/min between 20 °C and 150 °C, followed by a plateau of 2 h. Sections thicker than 12 mm are held at intermediate plateaus of 60 °C and 90 °C to minimize core-to-surface temperature gradients. Uneven postcure gradients create residual tensile stress at section roots and can open joint seams after final assembly. The finished test article is a wind-tunnel model with hollow internal stiffening cells and a surface finish compatible with oil-flow and pressure-sensitive paint measurement. For cryogenic wind tunnel use below 0 °C, a preliminary thermal soak and dimensional check on a sacrificial section are required because published data for this specific configuration are limited. Waste handling follows local photopolymer waste regulations because uncured portions remain reactive until fully postcured.
Autoclave layup tools printed from this resin are built as thick-section shells with internal lattice density adjusted to control heat capacity and vacuum line placement. The tool face is printed at 100 µm layer thickness for bulk sections and 50 µm around vacuum groove lips where edge sealing must be maintained. Because the filled acrylate system has low elongation at break, all vacuum groove intersections are filleted to prevent crack initiation along sharp recesses. After UV postcure, the tool is thermally postcured in a nitrogen-purged oven to 150 °C for 3 h, with ramp rates held to 0.3 °C/min across the glass transition region. Nitrogen purge reduces oxidative yellowing of the ceramic-filled surface during the postcure plateau. Tools are sealed with a filled epoxy fairing compound and coated with a semi-permanent release system compatible with carbon fiber laminates. Autoclave cycles at 120 °C to 150 °C and 6 bar internal pressure impose cyclic thermal and mechanical stress on the vacuum sealing lands. Cyclic thermal expansion mismatch between the ceramic-filled photopolymer tool and the carbon fiber laminate is characterized using coefficient of thermal expansion data measured per ASTM E831. Tool designers compensate for this mismatch by applying negative dimensional offsets to critical part datums. At cure temperatures above 120 °C, tool surfaces can soften selectively in areas where local heating exceeds the prior thermal postcure temperature; this failure mode appears as vacuum bag witness marks, surface dimpling, or fiber print-through on the cured laminate. The tooling output is a prototype autoclave tool for aircraft interior ductwork or motor sport body panels. Dimensional verification after each autoclave campaign is performed on a coordinate measuring machine according to ISO 10360-2. Because published fatigue data for this resin under high-pressure autoclave cycling are limited, such tools are designated for prototype trials rather than certified production runs. Operators inspect the tool for microcracks at sealing lands after any cycle that exceeds the specified dwell temperature by more than 5 °C. Amine-based release agents and cleaners are avoided because they can attack the crosslinked acrylate surface and reduce vacuum bag adhesion. The resin itself is supplied under REACH documentation; final laminate parts must meet their own applicable fire, smoke, and toxicity standards when installed in occupied aircraft compartments.
Short-run injection molding inserts are produced when prototype polyolefin parts must be molded in low quantities and hardened steel tooling is not justified. The insert geometry is designed with a shell thickness of 3 mm to 5 mm over internal conformal cooling channels and a channel diameter of 3 mm. The resin is printed at 50 µm layer thickness to capture gate and runner details, and supports are placed away from parting surfaces to reduce post-processing damage. Thermal postcure follows a peak of 150 °C for 2 h, but the insert is not expected to withstand the full heat deflection temperature of the filled polymer under injection pressure. Molding trials are conducted on vertical injection machines with clamp force below 50 t. Melt temperatures for unreinforced polypropylene are set between 200 °C and 230 °C. The first-shot thermal shock generates surface microcracks at sharp gate edges when the local temperature differential exceeds the thermal stability boundary. Gate geometries are redesigned with radiused transitions and no sharp corners. Ejector pin locations are printed as through holes, and inserts are backed with a machined steel support frame to distribute clamp force. Semi-permanent mold release agents are favored over silicone oil sprays because silicone migration fouls conformal cooling channels and changes heat transfer rates. Cycle counts are not standardized across molders because melt temperature, cooling efficiency, and injection speed vary widely. Dimensional verification of inserts before and after trials is performed on a coordinate measuring machine according to ISO 10360-2. Published data for this specific resin under high-speed injection molding cycles are limited; molders begin with low shot counts and inspect gate regions for crack initiation after each campaign. This practice limits the insert to prototype and single-batch production, not continuous manufacturing. The terminal output is a mold insert that yields molded parts with shape fidelity acceptable for functional testing but not for final part qualification under customer-specific metrology standards. The resin is not formulated as a food-contact material under 21 CFR 177, and the inserts are not used for medical device housings requiring ISO 10993 compliance.
Thermoforming masters face a thermal mismatch between the ceramic-filled photopolymer and heated thermoplastic sheet at contact temperatures between 100 °C and 160 °C. The master is built as a closed shell with wall thickness at least 4 mm to resist clamping pressure and repeated sheet contact. A sparse internal lattice of 2 mm cell spacing is generated under the forming surface to prevent surface sag during preheat. Thermal postcure is performed to 150 °C for 2 h to stabilize the polymer network before the first contact cycle. The as-built surface is sealed with a two-component epoxy filler and wet-sanded with 320-grit abrasive to reduce layer lines. Final polishing to 0.2 µm to 0.4 µm Ra is verified with a stylus profilometer according to ISO 4287. Vacuum vent holes are drilled into deep draw regions with diameters between 0.5 mm and 0.8 mm. The distance between vent holes is reduced below 25 mm in concave pockets to prevent trapped air from causing local thinning in the formed part. Ceramic heater preheat zones are monitored with an infrared pyrometer to keep the master surface below 160 °C; excursions above this threshold induce localized softening and imprinting of support pads or vent hole edges. The downstream part is a thermoformed article from high-impact polystyrene or amorphous polyethylene terephthalate with wall thickness controlled by plug geometry and sheet temperature profiles. Operators remove the master from the machine after each shift and measure critical dimensions with a non-contact scanner. Drift greater than 0.1 mm triggers resurfacing or replacement of the master. Master life is expressed in pilot-run campaigns rather than a fixed cycle count because draw depth, sheet gauge, and preheat profile vary by part design. Published data for long-term deflection under repeated thermoforming loads are limited, so tooling engineers rely on dimensional revalidation after each campaign. Food-contact certification is not conferred by the master; if thermoformed packaging is intended for food contact, the final article must be separately validated under 21 CFR 177 or an equivalent national positive list. The master is stored away from direct ultraviolet light to prevent secondary photopolymerization and surface dimension shift between production runs.
Assembly fixtures used in selective soldering and adhesive staging lines are produced from the resin where local temperatures can reach 180 °C for short contact times. The fixture is printed with a solid base thickness of 8 mm and component pockets offset by the expected thermal expansion of both the fixture and the assembled substrate. Thermal postcure achieves dimensional stabilization at 150 °C for 4 h in a forced-air oven. Fixture mounting points are isolated with steel bushings and floating washers to avoid bending stress as the fixture expands during the solder preheat stage. The pocket clearances are designed by measuring the coefficient of linear thermal expansion of the postcured resin according to ISO 11359-2 and applying the temperature rise from room ambient to the local peak. Where the cumulative positional error exceeds 0.15 mm across a 200 mm pocket array, the fixture is split into smaller segments to decouple expansion. This threshold is critical because surface-mount leads and flexible connectors demand placement accuracy within narrow windows. The deployed fixture is a line-specific workholder that positions printed circuit boards or flex circuits during solder paste printing, placement, and reflow. Process engineers measure fixture flatness before deployment on a granite surface plate; values above 0.1 mm per 300 mm are corrected by shimming or resurfacing. Alkaline cleaning agents are avoided because they can attack the filled acrylate surface and alter pocket dimensions. Thermocouple junction repeats on replicated fixtures are recorded and associated with a fixture serial number to detect batch-level postcure variation. Published data for repeated thermal cycling under production solder reflow conditions are limited; the fixture is therefore assigned to trial and small-lot assembly rather than continuous three-shift production without interim inspection. No-clean flux chemistries are evaluated on a sacrificial pocket insert before line deployment because some flux activators can penetrate the surface and reduce mechanical strength.
Reference bodies for structured-light scanning and optical dimensional inspection are printed when a dimensionally stable, opaque white surface is required to reduce contrast errors on complex geometries. The part is built at 50 µm layer thickness with orientation selected to keep critical datum features on the up-facing surface. Thermal postcure follows a 150 °C schedule to remove uncured monomer gradients that would otherwise cause dimensional drift during storage. After postcure, the reference body is left uncoated if the scanner uses a blue-light projector because the as-built surface supports diffuse reflection without additional powder. For laser scanners, a thin matte conditioning spray is applied to suppress specular peaks from semi-gloss feature edges. The reference body is then measured on a coordinate measuring machine using ISO 10360-2 to establish a baseline before field use. Acceptance criteria follow VDI/VDE 2634 Part 2 for optical 3D measurement of freeform surfaces; localized deviations above 0.03 mm are marked and excluded from scanner recalibration routines. The end use is a calibration artifact employed to verify scanner accuracy in tool rooms and metrology laboratories. Storage is specified away from direct sunlight and high-humidity environments because absorbed moisture and secondary photopolymerization can shift surface geometry by several micrometers over time. This segment is not intended for certified gauge calibration under ISO 17025 unless the artifact is independently verified and issued with a certificate by an accredited laboratory. Published data for long-term dimensional stability of this resin in uncontrolled metrology environments are limited; operators condition the artifact at 20 °C ± 1 °C and 50 % ± 10 % relative humidity for 24 h before use. The artifact is not subjected to solvent wiping because solvent uptake can alter surface stress state and cause local curvature change.
Конкурентоспособные цены на DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure, которые соответствуют вашему бюджету - гибкие условия и индивидуальные котировки для каждого заказа.
Для получения образцов, цен или более подробной информации свяжитесь с нами по адресу +8618136850665 или отправить по почте admin@ascent-chem.com.
Мы ответим вам как можно скорее.
Телефон: +8618136850665
Электронная почта: admin@ascent-chem.com
Гибкие условия оплаты, конкурентоспособные цены, первоклассное обслуживание — обращайтесь прямо сейчас!
DSM Somos PerFORM Reflect Stereolithography Polymer, Thermal Postcure, is a ceramic-filled photopolymer resin supplied for 355 nm stereolithography systems. The resin is distinguished from unfilled SL grades by a particulate mineral phase that lowers linear shrinkage, reduces the coefficient of linear thermal expansion, and raises heat deflection temperature after a mandated two-stage UV and thermal postcure. Manufacturer release documentation identifies the product as a stiff, low-elongation material intended for aerodynamic test articles, high-temperature composite tooling, investment casting patterns, and short-run injection mold inserts. The designation “Thermal Postcure” indicates that the published mechanical and thermal values are valid only after green parts have been UV flood-cured and then ramped through a forced-air oven cycle. Processing documents for the PerFORM family state that green-state parts retain insufficient crosslink density for elevated-temperature service; components placed into service without the postcure step fail by creep and surface softening at temperatures well below the published HDT.
The values in Table 1 are representative of supplier technical datasheets for specimens built in the X-Y plane at 50 μm or 100 μm layer thickness and tested after the specified postcure. Test methods are the supplier-reported standards for the PerFORM Reflect product line.
| Property | Test method | Typical postcured value |
| Tensile strength at break | ASTM D638-14 | 65–72 MPa |
| Tensile modulus | ASTM D638-14 | 9.8–10.5 GPa |
| Elongation at break | ASTM D638-14 | 0.8–1.3% |
| Flexural strength | ASTM D790-17 | 115–135 MPa |
| Flexural modulus | ASTM D790-17 | 9.5–10.5 GPa |
| Notched Izod impact | ASTM D256-10 | 14–20 J/m |
| Heat deflection temperature at 0.46 MPa | ASTM D648-18 | 280–320 °C |
| Heat deflection temperature at 1.82 MPa | ASTM D648-18 | 240–270 °C |
| Coefficient of linear thermal expansion, 25–100 °C | ISO 11359-2:2021 | 35–45 μm/m/°C |
The low elongation at break defines the product as a rigid, brittle polymer; designs must avoid snap-fit geometries and sharp notches. The high HDT values cannot be reproduced without postcure; supplier literature does not define elevated-temperature performance for UV-only parts, and laboratory measurements of unpostcured specimens are limited. The CLTE range is closer to aluminum than to unfilled SL resins and is the primary reason for use in composite mold tooling. Mechanical properties are build-plane dependent. Z-axis tensile strength and elongation are lower than X-Y values because interlayer boundaries remain local discontinuities despite postcure. Supplier datasheets may report only X-Y values; for load-bearing tools, through-thickness tensile modulus should be measured by ASTM D638-14 on vertically built coupons. The filler phase reduces postcure shrinkage but does not eliminate anisotropy; orientation-specific validation is required for thin ribs, bosses, and pressure-bearing surfaces.
On production-scale stereolithography platforms such as 3D Systems Viper si2 SLA, ProX 800, and comparable 355 nm solid-state laser systems, the filled resin requires conservative recoat settings. The supplier processing window for vat temperature is commonly 28–32 °C, and blade speeds are reduced by 20–50% relative to unfilled resins. The high filler loading raises low-shear viscosity to 2,000–4,000 mPa·s at 30 °C; because the material is shear-thinning, the viscosity measured at 1 s⁻¹ does not fully describe behavior at recoat blade shear rates. Filler settling during overnight idle periods can create a vertical compositional gradient, and manufacturing units report higher elastic modulus scatter in the first builds after idle unless the vat is recirculated or manually stirred for at least 15–30 min before starting. The recoat blade itself accumulates mineral filler at the meniscus over extended runs; operator inspections at 8 h intervals are commonly used to remove hard agglomerates before they produce surface streaks.
Machine qualification for filled resins begins with laser power and scan speed adjustments. On a 355 nm laser platform, scan exposure is typically increased by 15–35% relative to low-viscosity unfilled resins to compensate for light scattering, but the exact offset depends on layer thickness and particle content. Recoater systems using a vacuum-assisted or carbon-fiber blade are preferred; standard metal blades show accelerated edge wear. Vat level control is critical because the high density of the ceramic filler combined with low polymer viscosity at 30 °C creates a meniscus that can trap air bubbles. Air entrapment at the blade meniscus produces microvoids that become crack initiation sites in thin-wall sections. Degassing the resin for 15–30 min before use and avoiding pour-induced bubbles are standard production controls.
The material is selected when thermal dimensional control and modulus retention are more important than ductility. In composite tooling, postcured PerFORM Reflect inserts are used for carbon-fiber/epoxy prepreg cure cycles with tool temperatures in the 120–150 °C range; the CLTE of 35–45 μm/m/°C reduces panel distortion when the tool is restrained by steel backing plates. Dimensional tolerance checks after vacuum-bag debulk and autoclave cure follow tooling-specific inspection plans; published autoclave durability data for this exact formulation are limited, and unsupported vertical walls above 5 mm in section should be evaluated for creep at temperature. For aerodynamic test articles, the high HDT allows short-duration exposure to stagnation heating without the softening observed with unfilled SL resins. Postcured parts are machinable by CNC milling, drilling, and polishing; however, the brittle matrix requires sharp tooling and low feed rates to avoid edge chipping at thin trailing edges.
Thermal postcure is executed in a forced-air oven with controlled ramp and soak segments. Equipment-specific protocols for the PerFORM family specify an initial low-temperature hold to relax residual stress, followed by a higher-temperature segment to complete thermally activated crosslinking. Published exact ramp rates and soak temperatures for PerFORM Reflect are limited; typical PerFORM family ovens are set in the 120–160 °C range for total postcure times of 2–4 h. During the ramp, the loss modulus decreases and thin sections can warp; parts should be supported on a flat tooling plate or left on sacrificial supports until cooling is complete. If the oven overshoots the upper set point by more than 10 °C, localized surface oxidation may occur and dimensional accuracy may shift in large flat specimens. Thermocouple-mapped ovens with forced-air circulation are required for batch-consistent results. Postcured parts are cleaned with isopropanol in a ventilated wash station before thermal processing; residual alcohol trapped in porous surfaces should be dried for at least 30–60 min before ramping to avoid surface blistering.
Oven loading pattern influences the actual part temperature. Dense tooling plates reach set point later than thin wind tunnel skins; thermal lag between thermocouple and part surface can exceed 20 °C during ramp. Data loggers placed in sacrificial holes are recommended for tools thicker than 10 mm. Postcure under nitrogen or with limited oxygen is not required by the supplier, but air circulation should prevent hot spots. Gloss changes on upper surfaces are a field indicator of surface oxidation; if gloss changes more than 5 GU on a 60° glossmeter, oven temperature uniformity should be verified per ASTM E145-19.
The filled photopolymer exhibits reduced optical penetration depth relative to transparent SL resins because the ceramic particles scatter the 355 nm laser beam. The Beer–Lambert cure depth model is modified by scattering; effective penetration depth decreases as filler loading increases, and layer adhesion at 50 μm requires higher exposure than the settings used for WaterShed XC 11122. Process parameters from unfilled resins are not transferable. Overexposure produces lateral broadening of the cure region, which can close undercut features and generate dimensional growth on small holes and slots. Underexposure after idle periods, when filler has settled, produces weak interlayer adhesion and delamination during postcure. Cure inhibition is observed only when the vat is contaminated with moisture or solvent; the resin should not be processed at ambient relative humidity above 60%. Batch-to-batch viscosity and filler content are controlled by the supplier, but storage in sealed opaque containers at 20 ± 5 °C is required to prevent moisture uptake and photoinitiator degradation.
Compared with unfilled stereolithography polymers, PerFORM Reflect trades ductility for stiffness and thermal stability. Table 2 lists representative supplier datasheet comparisons. The unfilled materials are suitable for snap-fit prototypes and fluid-flow models but are not recommended for tool surfaces above 80 °C. PerFORM Reflect differs from original Somos PerFORM in filler packaging and final surface color; original PerFORM is selected for similar high-temperature use but may require additional surface finishing. Compared with 3D Systems Accura Bluestone, PerFORM Reflect is typically selected when a white or light-scattering surface is desired and when elevated postcured HDT is the primary acceptance criterion. Published direct comparison data at identical layer thicknesses and build orientations are limited; users should qualify the specific platform and postcure schedule with a design of experiments before production use.
| Material | Tensile modulus | HDT at 0.46 MPa | CLTE | Elongation at break |
| Somos PerFORM Reflect | 9.8–10.5 GPa | 280–320 °C | 35–45 μm/m/°C | 0.8–1.3% |
| Somos WaterShed XC 11122 | 2.5–2.8 GPa | 50–55 °C | 85–95 μm/m/°C | 12–20% |
| Somos NeXt | 2.3–2.7 GPa | 50–60 °C | 90–100 μm/m/°C | 15–22% |
Safety and regulatory handling follow the supplier safety data sheet. The uncured resin is classified as a skin and eye irritant; nitrile gloves, splash goggles, and local exhaust ventilation are required during vat charging, part removal, and sanding of cured parts. The thermally postcured solid is stable to handling but is not certified for food contact or medical implant use under FDA 21 CFR 177 unless the end user performs additional validation. REACH and RoHS declarations should be requested for the specific lot, because filler particle size distribution and photoinitiator content can vary between batches. Aerospace applications may require outgassing screening per ASTM E595-15; published TML and CVCM values for this specific grade are limited and must be determined on postcured specimens representative of the final build orientation and surface finish.