| Код ТН ВЭД | 664030 |
Как аккредитованный завод DSM Somos ProtoGen™ 18920 Liquid Photopolymer, UV Postcure, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
| Упаковка | Packaged in a 5 kg light-blocking plastic container, DSM Somos ProtoGen™ 18920 Liquid Photopolymer, UV Postcure, sealed against UV exposure. |
| Погрузка контейнера (20-футовый контейнер) | 20′ FCL: palletized drums of DSM Somos ProtoGen™ 18920 Liquid Photopolymer, UV Postcure, loaded upright, secured, shaded, protected from heat/light. |
| Доставка | DSM Somos ProtoGen™ 18920 Liquid Photopolymer, UV Postcure, is typically not regulated for transport under DOT/IATA/IMDG. Ship in original, tightly sealed, opaque containers, kept cool, dry, and away from UV light/heat. Use absorbent packing and spill containment; consult the SDS and carrier for final classification. |
| Хранение | Store in original, tightly closed containers in a cool, dry, well-ventilated area, protected from direct sunlight and UV light. Maintain 18–25°C (65–77°F); avoid heat, sparks, flames, and freezing. Keep away from oxidizers and incompatible materials. Use secondary containment. Keep containers upright and labeled. Do not store near food, drink, or feed. Follow SDS and local regulations. |
| Срок годности | Shelf life is 12 months when stored unopened in original container, protected from light, at recommended storage temperatures per manufacturer. |
In vacuum casting cells that support low-volume automotive and industrial equipment programs, ProtoGen™ 18920 is loaded into a stereolithography vat as a 100% solids, single-component liquid photopolymer; no reactive diluent, solvent, or monomer top-up is added because any reduction in formulation viscosity below the supplied condition shifts the critical exposure threshold and changes the recoater blade's wetting behavior. The only vat adjustment is a controlled virgin/reclaim blend. Reclaim filtered through a 25 µm stainless steel screen is held at or below 20 wt% to prevent particle-induced laser scattering and viscosity drift; published manufacturer guidance for this blend ratio is limited, so in-house viscosity and particle checks are required before each build. Compliance in this tooling application is anchored to dimensional and surface outputs rather than material certification: tolerance verification follows ISO 2768-1 class m and ISO 2768-2 class K, while the tooling shop's quality system is commonly operated under ISO 9001:2015. The downstream process begins with building the master pattern at 0.05 mm or 0.10 mm layer thickness on a 3D Systems Viper si2 or ProX 800 stereolithography platform equipped with a 355 nm solid-state laser; the finer layer setting is selected for bosses, ribs, and textured surfaces because stair-step height is reduced, but build time increases. After platform removal, the pattern is washed in tripropylene glycol monomethyl ether or isopropanol in a dual-tank ultrasonic bath, dried with low-pressure air, and transferred to a UV postcure chamber fitted with 365–405 nm fluorescent lamps. Postcure duration is calibrated to section thickness: thin-walled masters below 3 mm are typically exposed for 30–45 min per side, while thicker bosses and flanges require 60 min or more per side to eliminate residual methacrylate species. Residual uncured monomer at the pattern surface inhibits platinum-catalyzed addition-cure RTV silicone; a wipe test with isopropanol after postcure should leave no visible amber transfer. The postcured master is then mounted to a parting-line board, coated with a silicone-compatible release agent, and encapsulated by a tin-catalyzed or platinum-catalyzed RTV silicone to produce mold cavities. Terminal product types include polyurethane vacuum-cast intake manifold prototypes, gear housing prototypes, instrument panel bezels, and elastomeric grommet prototypes produced in shot sizes from 0.5 kg to 5 kg.
The operational boundary for ProtoGen™ 18920 in automotive assembly jigs is set before any UV postcure occurs. In the green state, immediately after removal from the stereolithography platform, the polymer network has reached only a fraction of its final crosslink density; jig bodies with long unsupported spans can creep under their own mass during solvent washing if the part is not fixtured. For this reason, the downstream manufacturing sequence begins with a build orientation that keeps the largest flat reference face parallel to the recoater blade and places support structures on non-critical surfaces. The resin is used at 100% solids without thinners or fillers; adding fumed silica or mineral fillers to reduce green-state creep is not recommended because non-reactive particles interfere with the 355 nm laser cure, lower the resin's penetration depth, and create anisotropic shrinkage. Compliance is governed by automotive tooling rather than part production: the jig manufacturer's quality system is commonly audited to IATF 16949:2016, while dimensional verification of the printed jig follows ISO 2768-1 class f and ISO 2768-2 class H for locating holes and datums. Mechanical verification uses flexural test coupons printed on the same build and tested under ASTM D790-17 after the same postcure cycle as the jig; coupons are conditioned at 23 °C and 50% RH according to ISO 291 before three-point bending. Washing is performed in isopropanol or tripropylene glycol monomethyl ether in an indexed ultrasonic bath, followed by forced-air drying at 40–50 °C for 30 min to remove residual solvent from blind holes and clamp slots. UV postcure is conducted in a reflective chamber fitted with 365 nm fluorescent lamps; the chamber's irradiance is measured with a calibrated radiometer before production lots, and low-irradiance bulbs or uneven chamber loading produce tacky surfaces and lower flexural modulus. After postcure, the jig body is machined on a three-axis CNC mill to create locating holes, insert steel or brass bushings with H7 tolerance, and attach toggle clamps or spring plungers. Terminal product types include drill templates, go/no-go check gauges, contour trace gauges, and robotic end-of-arm positioning fixtures used in body-in-white assembly stations.
When aerodynamic verification models are sectioned, sanded, and coated after stereolithography, the dominant process conflict is not initial build accuracy but the trade-off between stair-step smoothing and dimensional erosion. ProtoGen™ 18920 enters this application at 100% solids as the stereolithography vat charge; no solvent is added, but post-print surface preparation includes a high-build polyurethane primer applied at a dry film thickness controlled by a wet-film gauge. Published data for the optimum primer thickness on this specific resin is limited, so the coating system is typically validated on a sacrificial model section before production parts are prepared. Compliance for wind tunnel models is driven by aerodynamic data quality rather than material certification: dimensional checks follow ISO 1101 for geometric tolerancing, and surface texture is assessed using ISO 21920-2:2021 profile parameters after final sanding. The downstream process starts with building the model in sections at 0.05 mm layer thickness on a 355 nm stereolithography platform; sections are aligned with carbon fiber or steel dowel pins and bonded with epoxy adhesive. After assembly, the model is washed in isopropanol, UV-postcured under 365–405 nm lamps until no residual tack remains, and then hand-sanded from 120 grit to 600 grit using orbital and block sanders. Sanding heat and pressure can locally exceed the polymer's deflection temperature, so low-speed orbital tools and frequent cooling pauses are specified; excessive local heating produces surface smearing and dimensional distortion. After sanding, the model is primed, wet-sanded, and inspected with a portable stylus profilometer to confirm that surface roughness meets the wind tunnel facility's boundary-layer turbulence limit. Terminal product types include aerodynamic test models for front wings, rear wings, underbody diffusers, body panels, and aerospace control surface prototypes used in low-speed wind tunnel campaigns. The material is not suitable for high-temperature wind tunnel sections above 60 °C unless active cooling is provided; published data for elevated-temperature aero load performance of this specific resin is limited.
The use of ProtoGen™ 18920 for consumer electronics snap-fit prototype housings exposes a material limitation that must be managed during design: the UV-postcured network is notch-sensitive, and sharp corners at the base of cantilever snaps can initiate brittle fracture under repeated assembly or drop testing. The resin is used at 100% solids in the stereolithography vat without elastomer blending or plasticizer addition; attempts to modify the formulation at the vat level are not recommended because they alter the reaction kinetics of the 355 nm laser cure and create uncured pockets. Compliance for prototype validation demands mechanical testing rather than material certification: drop and shock sequences are performed according to IEC 60068-2-27, while dimensional checks of snap geometries follow ISO 2768-1 class f. RoHS Directive 2011/65/EU documentation must be requested from the supplier for any prototype that enters a consumer electronics product development process; the photopolymer is not a direct substitute for UL-rated injection-molding thermoplastics in production housings. The downstream process builds the housing at 0.05 mm layer thickness to resolve snap-hook lips and retention ribs; after washing in isopropanol and UV postcure under 365–405 nm lamps, support structures are removed and contact surfaces are hand-finished with 600–1200 grit abrasives. Heat-set threaded inserts are installed at 180–200 °C with a soldering station or an ultrasonic insertion press only after a test on a scrap section, because localized heat can soften or crater the postcured polymer. Terminal product types include smartphone prototype housings, wearable device enclosures, laptop hinge bezels, remote control housings, and earbud charging case prototypes subjected to iterative snap-fit and drop validation.
For non-implantable medical device prototyping, the two-stage modulus evolution of ProtoGen™ 18920 from green state to UV-postcured state must be integrated into surgical planning model approvals and instrument handle evaluations. The photopolymer is used at 100% solids as the vat charge; no sterilization-enhancing additives or antimicrobial agents are compounded into the resin. A formulation addition ratio therefore does not exist in the traditional compounding sense; instead, the build is controlled by virgin/reclaim ratio, with filtered reclaim limited to 20 wt% to maintain laser cure consistency. Compliance for medical device prototyping is a quality-system requirement, not a material biocompatibility claim: prototype fabrication is typically governed by ISO 13485:2016 procedures, and risk documentation follows ISO 14971:2019. If the prototype will contact tissue, blood, or mucosal surfaces, a supplier statement of ISO 10993-1:2018 evaluation must be obtained; absent such documentation, the part must be labeled as non-patient-contact and used only for design review or surgical planning. The downstream process starts with segmentation of CT or DICOM imaging data to create a digital surface mesh, followed by building at 0.05 mm layer thickness on a 355 nm stereolithography system. After build completion, the part is washed in isopropanol, UV-postcured under 365–405 nm lamps, and inspected for residual uncured monomer by solvent wipe test. Terminal product types include anatomical replicas for surgical planning, orthopedic instrument handle prototypes, endoscopic device housing mockups, and patient-specific bone models used for surgeon communication. Autoclave, ethylene oxide, or gamma sterilization cycles are not routinely validated for this material; any sterilization step requires separate testing and documentation because elevated temperature and ionizing radiation can alter the network and produce surface tack or dimensional drift.
When ProtoGen™ 18920 is used as a stereolithography pattern for investment casting of prototype impellers, valve bodies, and pump casings, the critical process boundary is the burnout furnace ramp profile above 700 °C. The liquid photopolymer is introduced into the vat at 100% solids without wax blending; foundries attach wax runners, gates, and risers to the completed SLA pattern using conventional hot-wax tools. Compliance in this application is governed by foundry dimensional output rather than polymer certification: casting tolerances are evaluated under ISO 8062-3, and the foundry's quality system is commonly audited to ISO 9001:2015. The downstream process begins with building a hollow pattern or a solid pattern with internal drain holes at 0.10 mm layer thickness on a 355 nm stereolithography platform; hollow sections reduce thermal expansion stress during burnout but must be large enough to allow uncured resin drainage before postcure. After the build, the pattern is washed, UV-postcured under 365–405 nm lamps until no tack remains, and then mounted on a wax tree. The tree is shelled with alternating zircon and colloidal silica slurry coats; each coat is dried and hardened before the next is applied. During the burnout phase, the shell is heated in an autoclave or flash-fire furnace. The decomposition of the photopolymer generates volatile species and carbonaceous residue; if the ramp rate through 200–400 °C is too fast, internal pressure from volatilization can crack the ceramic shell. Foundries therefore run a prolonged hold at 300–400 °C before ramping to 700–900 °C. The residual ash content of this specific resin in the shell cavity must be characterized by thermogravimetric analysis under ISO 11358-1 before production runs; published data for this specific configuration is limited, so each foundry should validate a loss-on-burnout procedure. Terminal product types include prototype stainless steel, carbon steel, and aluminum alloy cast impellers, valve bodies, pump casings, and manifold components for low-superheat foundry trials.
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DSM Somos ProtoGen™ 18920 Liquid Photopolymer, UV Postcure is formulated for 355 nm laser-scanned stereolithography platforms in which parts are built layer-by-layer and subsequently stabilized by ultraviolet postcure. The grade belongs to the Somos ProtoGen family, which is commonly positioned for polypropylene-like functional prototypes and master patterns requiring dimensional repeatability after secondary processing. In production-scale operations, the resin is processed at a vat temperature of 30 °C ± 2 °C, with layer thickness selections of 0.050 mm, 0.100 mm, or 0.150 mm depending on feature size, surface-finish constraints, and vertical accuracy. Machines using galvanometer-controlled scanning and a nominal wavelength of 355 nm, typified by the 3D Systems Viper si2 and larger-frame SLA 5000 series, are common reference platforms. The material must be shielded from ambient UV sources; storage in the original sealed container at 15 °C to 30 °C is generally required to preserve polymerization response and prevent premature gelation.
Lot-to-lot repeatability in the ProtoGen 18920 vat begins with storage and fluid handling, not only with machine parameter sets. Resin stored below 15 °C may develop viscosity stratification and should be brought to 30 °C ± 2 °C without direct heating or open-flame sources. Depending on container volume, passive equilibration can require 2 h to 4 h; forced-air heaters are not recommended because localized skin heating may initiate dark polymerization at the container wall. Containers exposed to high-humidity environments should be kept sealed when not in use. Absorption of atmospheric moisture can shift the critical exposure dose and produce a tacky or powdery surface on the first layers after build startup. Gentle mixing is acceptable only if it does not generate bubbles; high-shear mixing can entrain air that appears as microvoids after recoating. Production sites operating in relative humidity above 60 % should evaluate predrying or dry-air purging of the resin handling area before the build is released.
Depth of polymerization in this resin is a function of the working-plane exposure energy rather than the programmed slice thickness alone. When the measured scan spacing exceeds the 1/e² beam width by more than 15 %, adjacent laser scan tracks may fail to form a continuous overlap, producing weak interlayer planes that are not visually obvious in the green part. Real-world solid-state SLA platforms with nominal laser output between 400 mW and 800 mW frequently deliver only 35 % to 60 % of nominal output at the vat surface after optics attenuation and quartz-window fouling. Periodic calibration with a 355 nm thermopile radiometer is therefore necessary before critical builds. Drift beyond 5 % from the baseline power measured at the last successful run is a standard trigger for inspecting the beam expander, galvo mirrors, and vat window before proceeding. These observations reflect production-scale SLA equipment behavior because machine configuration strongly affects the actual exposure dose delivered to the resin.
Recoat uniformity in the ProtoGen 18920 vat is determined primarily by the viscosity of the liquid resin at the build temperature and by the geometry of the recoater blade. If the resin temperature falls below 28 °C, viscosity rises enough to slow leveling after each recoater pass; blade skip marks and trapped air can then appear on the top build layer. On fixed-gap recoater systems using a 0.254 mm blade gap, the affected area may show a surface depression whose depth corresponds to the uncured resin that was not correctly displaced. If the vat temperature exceeds 32 °C, the induction time for dark polymerization shortens, allowing gel particles to form in stagnant regions of the vat. These particles can adhere to the part surface or create raised defects after multiple sequential builds. The industrial control window of 30 °C ± 2 °C is therefore not a convenience value; it balances viscosity reduction against the onset of premature polymerization in the vat.
On production-scale systems, recoat speed is generally set between 80 mm/s and 140 mm/s for large-area recoating. Blade acceleration is ramped so that the liquid meniscus behind the blade does not break and entrain air; a broken meniscus can generate voids whose lateral width exceeds 0.1 mm and whose location follows the recoater trailing edge. The optimum speed depends on resin lot viscosity, vat temperature, and recoater design. Operators should log the viscosity of each incoming lot at 30 °C using a rotational viscometer method such as ASTM D2196-20 or a cone-and-plate technique aligned to ISO 2884-2:2006. A lot-to-lot viscosity shift of more than 10 % relative to the preceding lot is a valid cause for recoat parameter adjustment, even if the resin remains within the supplier’s acceptance range.
When the green part is removed from the build platform, the photopolymer network remains intentionally underconverted; this preserves part ductility during support removal but leaves reactive groups that must be consumed during UV postcure. Excess liquid resin is first removed by sequential solvent cleaning. A primary bath of isopropyl alcohol with concentration above 90 % is common, followed by a second clean bath to avoid redeposition of diluted resin. Compressed-air drying at 2 bar to 4 bar removes solvent from recesses; air lines must be filtered to avoid oil contamination. A tacky residue after drying indicates that the solvent bath is saturated or that the part was not fully drained. If tripropylene glycol monomethyl ether is used as an alternative, the vented cleaning station must be configured for its lower vapor pressure and longer evaporation time.
UV postcure chambers for this product class typically use metal-halide or high-pressure mercury lamps with emission between 320 nm and 420 nm. Parts are placed on rotating or indexing trays to distribute exposure across all surfaces. Total UV dose measured in the UV-A band is usually held at 20 J/cm² to 40 J/cm² per exposed face. Doses below 15 J/cm² can leave heat deflection temperature and solvent resistance below the fully cured baseline; doses above 60 J/cm² can embrittle thin-wall areas and increase oxidation-driven yellowing. Postcure is exothermic, and thin-wall sections below 1.0 mm may warp when placed on dark metal trays that absorb incident energy and create thermal gradients. Sustained part-surface temperatures above 60 °C during UV postcure are generally outside the intended window for dimensionally stable patterns. Radiometer calibration should be performed against a UV source of known spectral output; lamp-hour counters alone do not verify that the correct dose reached the part surface.
Mechanical properties reported for DSM Somos ProtoGen™ 18920 must be interpreted according to specimen geometry, build orientation, postcure schedule, and conditioning environment. Producers of SLA photopolymer data typically follow the matrix shown in Table 1. The use of a single set of parameters without reporting build orientation can understate anisotropy and mislead comparisons with large-format industrial resins.
| Property | Standard/Method | Specimen/Condition | Unit |
|---|---|---|---|
| Tensile strength, elongation | ASTM D638-14 / ISO 527-2:2012 | Type I / 1B, crosshead 5 mm/min, 23 °C ± 2 °C, 50 % ± 5 % RH | MPa, % |
| Flexural modulus | ASTM D790-17 / ISO 178:2019 | Three-point bend, span 64 mm, crosshead 1.3 mm/min | MPa |
| Heat deflection temperature | ASTM D648-16 / ISO 75-2:2013 | Edgewise at 0.45 MPa, heating rate 2 °C/min | °C |
| Notched Izod impact | ASTM D256-10 / ISO 180:2019 | Method A, notch radius 0.25 mm, 23 °C ± 2 °C | J/m, kJ/m² |
| Water absorption | ASTM D570-98 | 24 h immersion, 23 °C | % |
| Hardness | ASTM D2240-15 | Shore D, 3 s reading | Shore D |
Published numerical values for ProtoGen 18920 are not reproduced here because open-source summaries often lag behind formulation revisions and may omit orientation-specific data. The supplier’s current technical datasheet remains the authoritative source for absolute property boundaries; the matrix above is supplied only to define the test conditions under which such values should be compared.
A deficient postcure cycle may not be apparent from Shore hardness measurements alone. Parts can appear solid but retain an underconverted core or interlayer region that fails under service conditions well below expected tensile stress. In many SLA photopolymers, an undercured interlayer is most clearly observed as an increase in the ratio of horizontal to vertical tensile strength; anisotropy ratios above 1.5 have been documented in production audits when the postcure dose was below the critical threshold. Isopropyl alcohol wipe testing can identify residual liquid or lightly crosslinked resin on the surface, but it does not quantify conversion depth. Dynamic mechanical analysis on fully cured and deliberately undercured specimens indicates that storage modulus at 50 °C may be lower by 20 % or more when UV radiometer calibration has drifted by 10 %. This modulus deficit is not recoverable by subsequent solvent cleaning or surface priming.
Load-bearing applications expose underconverted interlayer regions that routine Shore hardness measurements miss. The first visible sign is often a whitening or delamination at support-scar locations after the part is subjected to bending or impact. Because the UV postcure step is intended to increase crosslink density through the full wall thickness, a short or shadowed postcure cycle leaves the core softer than the surface. On thick sections above 6 mm, postcure uniformity is particularly sensitive to tray placement and part orientation; underside surfaces facing the tray may receive less than 50 % of the incident dose unless parts are rotated. Production facilities that rely on dynamic mechanical analysis or differential scanning calorimetry use those techniques to verify that the glass transition or storage-modulus baselines are reached before releasing functional prototypes. A single bulk property value is insufficient for process verification because residual underconversion can be localized in the interlayer region.
Process calibration for scanning-laser SLA platforms is summarized in Table 2. The tolerances listed are industrial control limits, not absolute resin property limits; they provide a starting point for process-stability assessment on UV-laser machines.
| Variable | Typical Industrial Tolerance | Observation Method |
|---|---|---|
| Vat temperature | 30 °C ± 2 °C | Calibrated thermocouple at vat perimeter |
| Laser power at vat surface | ±5 % of baseline | 355 nm radiometer |
| Recoat speed | 80 mm/s–140 mm/s | Machine parameter verification |
| UV postcure dose | 20 J/cm²–40 J/cm² per face | UV radiometer, 320 nm–420 nm band |
| Recoat blade gap | 0.254 mm nominal | Feeler gauge before build |
Typical production uses for DSM Somos ProtoGen™ 18920 include vacuum-casting master patterns, short-run enclosures, snap-fit demonstration parts, form-and-fit verification housings, and airflow-test components in which moderate dimensional stability after secondary processing is required. The grade is selected over lower-temperature general-purpose SLA resins when the part will undergo silicone molding, painting, or thermal forming of subsequent casting materials. However, users should not substitute ProtoGen 18920 data for ProtoGen 18120 or ProtoGen 18420 data without reviewing the current datasheet; the suffix designations correspond to different property balances, and open-source cross-comparisons frequently understate orientation and postcure effects. Published data for this specific configuration is limited for sustained load at temperatures above 75 °C and for long-term outdoor weathering; those applications require application-specific testing rather than direct datasheet transfer. The material should not be assumed to comply with FDA 21 CFR food-contact requirements, ISO 10993 biocompatibility requirements, or REACH/RoHS restrictions without current supplier documentation. Strong alkaline cleaning solutions above 50 °C and prolonged immersion in aggressive organic solvents should be treated as incompatibilities unless comparative chemical resistance data is supplied. Before silicone tooling compounds are used against the resin pattern, the specific platinum-catalyzed silicone should be tested for cure inhibition because partially postcured photopolymer residues at the surface can interfere with the silicone crosslinking reaction at the interface.