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Eastman Amphora™ SP1621 3D Polymer Powder

    • Название продукта: Eastman Amphora™ SP1621 3D Polymer Powder
    • Сайт Factroy: Округ Юду, Ганьчжоу, Цзянси, Китай
    • Запрос цены: admin@ascent-chem.com
    • Производитель: Ascent Petrochem Holdings Co., Limited
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    Спецификации
    Код ТН ВЭД 839742

    Как аккредитованный завод Eastman Amphora™ SP1621 3D Polymer Powder, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.

    Упаковка и хранение
    Упаковка Packaged in a 1 kg moisture-resistant, resealable container for safe storage and handling of Eastman Amphora™ SP1621 3D Polymer Powder.
    Погрузка контейнера (20-футовый контейнер) 20′ FCL container loading: palletized, shrink-wrapped bags of Eastman Amphora™ SP1621 3D Polymer Powder, secured for ocean shipment.
    Доставка Eastman Amphora™ SP1621 3D Polymer Powder is not regulated for transport by DOT, IMDG, IATA, or ADR. Ship in sealed, labeled containers to prevent moisture ingress and dust release. Store in a cool, dry, well-ventilated area away from ignition sources. Follow local regulations and the manufacturer’s SDS.
    Хранение Store Eastman Amphora™ SP1621 3D Polymer Powder in a cool, dry, well-ventilated area, away from direct sunlight, heat, sparks, flames, and moisture. Keep containers tightly closed to prevent dust generation and contamination. Avoid contact with strong oxidizers. Use proper grounding and local exhaust when handling. Protect from static discharge. Store at ambient temperature. Keep out of reach of children.
    Срок годности Eastman Amphora SP1621 3D Polymer Powder has a 24-month shelf life from manufacture when stored unopened in cool, dry conditions.
    Применение Eastman Amphora™ SP1621 3D полимерного порошка

    Eastman Amphora™ SP1621 3D polymer powder is dry-blended with recovered powder at a mass ratio of 60:40 for laser-sintered aircraft cabin air-distribution plenums, cable clamp assemblies, and seat-back close-out panels. The powder is conditioned at 70 °C for 4 h under a dew point of −40 °C prior to loading in a nitrogen-inerted powder-bed fusion system operating at an oxygen concentration below 1.5 vol%. Layer thickness is set to 0.12 mm on a 30 W CO₂ laser machine with a 200 mm × 200 mm × 200 mm build volume; the part-bed temperature is held 12–18 °C below the melting peak determined by differential scanning calorimetry at 10 K/min per ISO 11357-3. Laser energy density is adjusted to 0.08 J/mm³ for contour passes and 0.12 J/mm³ for hatch passes, and scan speed is reduced by 10 % when the cross-section area exceeds 50 mm². Sintered tensile coupons are conditioned for 24 h at 23 °C and 50 % RH before testing according to ASTM D638-14; the processor verifies batch-to-batch consistency by recording notched Izod impact values per ISO 180/A and density by ISO 1183-1. Finished duct sections must satisfy the 12 s vertical burn requirement of FAR 25.853(a) Appendix F Part I, with an average burn length not exceeding 152 mm and an afterflame time not exceeding 15 s; any drip that ignites cotton is a failure. Powder recovered from unsintered cake is sieved through a 150 µm mesh and added at the same 60:40 virgin-to-recovered ratio for the next build.

    What changes when SP1621 replaces glass-filled nylon in rail interior seat-back shells?

    Replacing glass-filled polyamide 12 with Eastman Amphora™ SP1621 shifts the powder-bed hold temperature downward and alters the refresh-rate ceiling because copolyester melt rheology differs from polyamide crystallization behavior. In a rail seat-back build, the target layer height is 0.10 mm, and the part-bed temperature is maintained within 8–12 °C of the crystallization onset measured on the second heat by ISO 11357-3; exceeding this window induces edge curl and part growth in unsupported overhangs. The component's fire-smoke-toxicity envelope is evaluated under EN 45545-2 Annex B for R22 interior surfaces, requiring smoke density measurements according to EN ISO 5659-2 with a Ds max value normally below 150 for HL2, and gas analysis per EN 17084 or NF X 70-100, with carbon monoxide yields below the stated 4-minute and 8-minute limits. A blend of 55 wt% virgin powder and 45 wt% recovered powder is used when the recovered fraction has been sieved to 140 µm and dried to less than 0.05 % moisture; higher recovered content increases melt-flow instability and produces visible porosity in thin-walled bosses. The end product is a fire-retardant seat-back shell and armrest cap, with integrally printed snap-fits and cable-routing channels, post-processed by glass bead blasting without chemical smoothing because solvent exposure can stress-crack the sintered walls.

    Custom ankle-foot orthosis shells are produced by scanning a patient leg model into a build volume where SP1621 powder is spread at 0.10 mm layer thickness. The laser parameters are adjusted to achieve a volumetric energy density of 0.12 J/mm³ with a scan spacing of 0.20 mm; this setting is machine-specific and must be revalidated after changing the optical window. A skin-contact device made from this powder must undergo cytotoxicity testing according to ISO 10993-5 and irritation testing according to ISO 10993-10; the supplier publication for SP1621 does not remove the manufacturer's obligation to qualify the finished device under ISO 10993-1, particularly if the orthosis is worn for more than 30 days. The sintered shell wall is designed with a nominal thickness of 3.2 mm and a lattice infill of 35 %; local thickenings above 6.0 mm should be avoided because they increase cooling-induced dross and reduce dimensional accuracy. The finished orthosis is sealed with a medical-grade polyurethane topcoat to limit moisture absorption and cleanability failure. Recovered powder is limited to 40 wt% for patient-contact builds, and the blend is homogenized in a tumble mixer for 20 min at 15 rpm before sieving.

    Application segmentIgnition/flame testSmoke/toxicity testMechanical verification
    Aircraft cabin air ductFAR 25.853(a), 12 s vertical burn, 152 mm burn lengthAITM 2.0002 or ABD 0031ASTM D638-14 tensile, ISO 180/A impact
    Rail seat-back shellEN 45545-2 R22, HL2EN ISO 5659-2 Ds max, EN 17084ISO 178 flexure, ISO 75-2 HDT
    OrthosisNot applicable unless oxygen-enrichedISO 10993-5, ISO 10993-10ASTM D638-14 tensile, ISO 527-2
    Electrical enclosureIEC 60695-11-10, IEC 60695-2-13Not specified for general useASTM D256 notched Izod, IEC 60112 CTI

    Investment casting pattern burnout and ash-residue thresholds

    Investment casting pattern production from SP1621 is viable for low-temperature alloys when the foundry demonstrates that total post-burnout residue remains below 0.01 wt% by ISO 3451-1. Patterns are built with perimeter walls of 1.5 mm and an internal honeycomb fill of 12 %; the outer surface is sealed with a microcrystalline wax blend before ceramic shell dipping. Burnout is conducted in a forced-air furnace ramped at 2 °C/min from 20 °C to 600 °C with a 2 h soak at peak temperature; the shell must be vented to prevent pressure rupture from evolved decomposition gases. Published data for this specific configuration is limited; therefore, a foundry must run differential scanning calorimetry and thermogravimetric analysis per ISO 11358-1 on each new lot of SP1621 to confirm the decomposition onset and ash content. The end product is a ceramic shell for aluminum A356 or stainless-steel small impellers, with the polymer pattern completely burned out before metal pour.

    When SP1621 is processed without nitrogen inerting for electrical enclosure prototypes

    When Eastman Amphora™ SP1621 is processed in an open-bed machine without nitrogen inerting, the oxygen concentration at the powder surface typically rises above 5 vol%, increasing yellowing and lowering impact strength. For electrical enclosure prototypes, the build chamber is therefore purged with nitrogen until the oxygen concentration is below 1.0 vol%; the bed temperature is held at 102–110 °C, and the laser power is increased by 8–12 % relative to polyamide 12 settings. Recovered powder fraction is held at 30 wt% because darkening from recycled copolyester affects comparative tracking index measurements. The sintered enclosure walls are tested for flame retardance according to IEC 60695-11-10 at the as-built thickness of 2.0 mm; the processor must request a thickness-specific rating certificate from the powder supplier, as published V-0 data may apply only to a particular thickness. Comparative tracking index is measured according to IEC 60112, and glow-wire ignition temperature is measured according to IEC 60695-2-13 for unattended household appliance applications. The end component is a low-volume electrical housing with integrated strain-relief slots and PCB standoffs, post-processed by vibratory finishing and sealed with a silicone-free conformal coating; silicone-free chemistry is specified to avoid contamination that would reduce adhesion in downstream bonding.

    Processing variableAircraft ductingRail seat-backOrthosisElectrical enclosure
    Layer height0.12 mm0.10 mm0.10 mm0.12 mm
    Part-bed temperature12–18 °C below melt peak8–12 °C above crystallization onsetMachine-specific, revalidate after optical window change102–110 °C
    Recovered powder fraction40 wt%45 wt%40 wt%30 wt%
    Oxygen limit1.5 vol%1.5 vol%1.0 vol%1.0 vol%

    Consumer drone air ducts and sensor brackets are built at a layer height of 0.10 mm with a 50 wt% recovered-powder fraction. The parts are printed without support structures; self-supporting overhang angles are limited to 45° from vertical to maintain surface finish. The duct wall thickness is set to 1.2 mm to balance stiffness and mass; the sintered parts are conditioned at 80 °C for 2 h to stabilize dimensions before metrology. Vibration resistance of motor mounts is verified under MIL-STD-810H Method 514.8, with a random vibration profile from 10 Hz to 500 Hz at 0.02 g²/Hz for 2 h per axis; this requirement is product-specific and not an inherent material rating. The end product is a ducted fan housing and an IMU bracket, both produced in single-build lots without tooling.

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    Сертификация и соответствие требованиям
    Более подробное введение

    Eastman Amphora™ SP1621 3D Polymer Powder is an amorphous copolyester powder supplied for powder-bed additive manufacturing, specifically laser-based powder bed fusion and high-speed multi-jet fusion platforms. The grade is positioned as a low-odor, styrene-free alternative to semicrystalline polyamide and acrylic powders, with a supplier-reported density of 1.20–1.24 g/cm³ per ISO 1183-1 and a controlled particle-size distribution for counter-rotating roller and blade spreading systems. The amorphous architecture removes the sharp melting peak used for calibration with polyamide 12; coalescence is governed by time-temperature behavior above the glass transition. Typical uses include functional housings, brackets, ducting, and short-run production tooling where dimensional stability and low moisture uptake are required. Published data for SP1621-specific processing windows on all machine platforms is limited; pre-production trials are required to establish build-chamber setpoints, laser energy density, and refresh ratio.

    Amorphous Copolyester Architecture Eliminates a Sharp Melting Plateau

    The absence of a semicrystalline melt endotherm changes the thermal control strategy on laser-sintering equipment. Quiescent bed temperature is maintained below the onset of viscous flow to prevent premature fusion of non-lased powder; build-chamber controllers that rely on polyamide 12 melt-peak indexing are therefore replaced by calibration against powder flow energy and tap density. In production-scale powder-bed systems, this shifts attention to a broad coalescence window rather than a narrow melt plateau. Supplier technical bulletins describe a processing window that is wider than semicrystalline polyamide but narrower than filled elastomers; machine-specific optimization remains necessary because infrared absorbers and bed preheat lamps interact with the powder’s near-neutral intrinsic color. The powder is suitable for CO₂ laser systems with nominal 30 W to 60 W output and for volumetric energy densities typical of unfilled thermoplastics. Published data for specific scan speeds and hatch spacings is limited; parameter development on a per-machine basis is required.

    What Distinguishes SP1621 from Semicrystalline Polyamide Powders?

    Polyamide 12 powders absorb atmospheric moisture at equilibrium values commonly reported in the range of 1.2–2.5% by mass per ASTM D570, whereas SP1621’s copolyester chemistry reduces equilibrium moisture uptake to a supplier-declared range below 0.5%. This difference directly affects powder flow, dimensional drift, and the frequency of pre-drying in humid production cells. Polyamide 12 also exhibits a melting peak near 186 °C, which produces a sharp drop in viscosity during fusion; SP1621 transitions through a broadening flow regime above its glass transition, resulting in lower residual stress accumulation and reduced curl on large flat sections. The styrene-free composition eliminates the odor signature associated with styrenic toners and extends the range of production environments in which the powder can be run without aggressive fume extraction. Mechanical property comparisons are given in the table below.

    In powder-bed fusion workflows, SP1621 is introduced as a dry powder with controlled fines content. The powder is spread on standard laser sintering and multi-jet fusion equipment; layer thickness is typically configured between 80 μm and 120 μm. Recycled powder is sieved through 150 μm mesh and blended with virgin powder at ratios determined by powder flow energy and melt-flow retention. Build failures on production lines are most frequently traced to moisture pickup above 0.3% or accumulation of sub-10 μm fines, which reduces spreader ridge stability and creates short-feed defects. Operators using enclosed conveying and desiccant dryers at 60 °C for 4 h before transfer to the hopper suppress these failures. Because the grade is amorphous, long-term retention of powder in a heated bed can raise bulk flow energy and produce part growth; bed temperature should be reduced by 5–10 °C when idle for more than 60 min. These operational limits are derived from production-scale powder-bed equipment behavior and require validation on the specific machine model in use.

    Powder Flow Energy, Particle-Size Boundaries, and Recoater Stability

    Powder flow energy is a more sensitive predictor of recoater stability than simple angle-of-repose measurement. In production cells with counter-rotating roller spreaders, the powder is metered into a dosing chamber at gaps of 0.5–1.0 mm; agglomerates larger than 250 μm create drag lines and disrupt layer uniformity. SP1621 is supplied with a controlled fines fraction, but attrition during pneumatic conveying can increase sub-10 μm particles. A lot that enters the machine with acceptable flow energy can fail after 3–5 build cycles if fines are not removed by sieving. The use of a 150 μm sieve is standard for polyamide powders, but SP1621’s lower particle density can make screen blinding more frequent when humidity exceeds 50%. Operators on production lines report that reducing the sieve deck angle and using ultrasonic screen excitation improves throughput without altering the particle-size distribution.

    Because SP1621 is amorphous, powder aging is dominated by physical particle attrition and oxidative yellowing rather than crystalline reorganization. Melt-flow retention after recycling is therefore a more relevant quality metric than differential scanning calorimetry melt enthalpy. The supplier’s recommended refresh ratio must be calibrated against melt-flow index measured by ISO 1133-1:2022 at 230 °C under 2.16 kg load; a reduction in melt-flow index greater than 25% from virgin powder indicates excessive residence time in the heated build chamber. Thermal aging in air at build-chamber temperatures near 100 °C can reduce part elongation before visible yellowing occurs. This creates a process conflict: higher bed temperatures improve interlayer fusion but accelerate oxidative aging. The operating window is therefore narrower than the broad amorphous coalescence envelope would suggest; production lots should be monitored with melt-flow index and notched Izod impact coupons at 24 h intervals during extended campaigns.

    To Process Without Moisture-Induced Agglomeration, Drying Must Precede Preheat

    The powder should be dried to a moisture content below 0.1% by ISO 15512 before processing. Open storage at relative humidity above 60% for more than 24 h requires re-drying at 60–70 °C for 4–6 h in a desiccant or vacuum dryer. Build-chamber preheat is adjusted to maintain the powder bed surface temperature within a narrow band; because SP1621 does not provide a melt-peak reference, operators use a bed-temperature ramp with powder flow energy measurements at 10 °C increments to identify the onset of particle stickiness. On production machines with non-contact infrared sensors, this onset is typically observed before the powder reaches its glass transition onset. The build chamber is then held below that temperature by a margin of 10–15 °C to allow for local laser heating. Additional cooling airflow over the recoater is recommended on systems with blade spreaders to prevent static charge accumulation and powder carryover. Low-odor processing does not eliminate the need for standard particulate filtration; however, the styrene-free decomposition profile reduces volatile organic compound load relative to styrenic powders.

    When Moisture Uptake Governs Dimensional Stability

    Parts built from SP1621 in a humid production environment retain dimensional stability better than polyamide 12 benchmarks because the equilibrium moisture content is lower. When parts are conditioned at 50% relative humidity and 23 °C for 40 h, the mass increase is less than 0.3%; by contrast, polyamide 12 components can exhibit mass increases exceeding 1.0% under identical conditions. This correlates with reduced water-induced plasticization and lower shift in flexural modulus after conditioning. The difference is most relevant for thin-walled enclosures with wall thicknesses below 2 mm, where moisture uptake in unreinforced polyamide can produce measurable changes in snap-fit retention and boss geometry. For environments with continuous water immersion or steam exposure above 60 °C, chemical compatibility testing under ASTM D543 is required; copolyesters generally tolerate short-term contact with dilute acids and aliphatic hydrocarbons but are not recommended for strong alkaline solutions at elevated temperature.

    Comparing SP1621, PA12, and TPU Under Identical Test Conditions

    Representative values are drawn from supplier technical bulletins for unfilled laser-sintered and multi-jet fusion grades. SP1621 values should be verified against the current lot certificate of analysis; polyamide 12 and TPU references are included solely to illustrate the property envelope under identical test conditions.

    Property and Test MethodSP1621 Representative RangeUnfilled PA12 ReferenceUnfilled TPU Reference
    Density, ISO 1183-11.20–1.24 g/cm³1.01 g/cm³1.10–1.25 g/cm³
    Tensile strength, ASTM D638-1445–50 MPa45–50 MPa25–35 MPa
    Tensile modulus, ASTM D638-141.9–2.2 GPa1.5–1.8 GPa0.02–0.05 GPa
    Elongation at break, ASTM D638-1410–20%15–30%300–500%
    Moisture uptake, 24 h, ASTM D570<0.5%1.0–2.5%0.2–0.5%
    Heat deflection temperature, 0.455 MPa, ASTM D648-1890–105 °C150–170 °C60–80 °C

    Mechanical property values for powder-bed parts are orientation-dependent. Type IV tensile specimens built in the XY orientation exhibit higher elongation than Z-oriented specimens because interlayer cohesion in a powder-bed fusion process is controlled by thermal penetration and layer time. When evaluating SP1621 against injection-molded copolyester datasheets, designers must use printed-specimen data, not resin data. Suppliers of powder-bed polyamides report as much as a 20–30% reduction in Z-direction tensile strength relative to XY; for SP1621, laboratory comparisons under the same build conditions show a smaller orientation gap due to the broad coalescence range and lower crystallinity. However, published data for specific machine models is limited; users should generate a three-build orientation matrix on the target platform before committing to production tooling.

    For Regulated Production Environments, the Crosswalk Is Not Optional

    The following matrix consolidates the standards most frequently required when qualifying SP1621 for production. Compliance is not implied; supplier documentation and lot-specific certificates of analysis must be reviewed.

    RequirementStandard or Regulation
    Tensile propertiesASTM D638-14
    Flexural propertiesASTM D790-17
    Notched Izod impactASTM D256-10(2018)
    Heat deflection temperatureASTM D648-18
    DensityISO 1183-1:2019
    Melt-flow indexISO 1133-1:2022
    Moisture contentISO 15512:2019
    REACH SVHC screeningRegulation (EC) No 1907/2006
    RoHS restricted substancesDirective 2011/65/EU, Annex II

    To Determine Whether SP1621 Fits a Low-Odor Production Cell

    Production cells with existing polyamide laser-sintering equipment can evaluate SP1621 by substituting the powder after a full hopper and filter cleaning. The changeover requires removal of residual polyamide 12 because mixing semicrystalline and amorphous powders alters coalescence behavior and can generate out-of-spec porosity. In observed production-scale runs, leftover polyamide dust inside the breakout station was a greater source of contamination than the powder inlet, producing visible glassy inclusions and variable tensile elongation. Dry-ice blasting and vacuum cleaning with HEPA-filtered capture are recommended before first use. Particulate exposure control remains mandatory; the supplier safety data sheet should be reviewed for local exposure limits. Because the grade is styrene-free and low-odor, process exhaust may be recirculated in some jurisdictions, but the facility’s air permit and ISO 45001 risk assessment should govern the final configuration.

    Short-run production tooling and protective equipment components are candidate applications when low moisture uptake and low odor are process requirements. In a manufacturing cell running a powder-bed machine with 100 μm layers, SP1621 can be substituted into existing nylon tooling workflows after cleaning and process calibration. Parts have been produced in configurations with snap-fit features, living hinges, and threaded inserts; however, published data for specific insert retention forces and hinge-cycle endurance is limited. The grade should not be combined with polyamide 12 powder residues, and the machine’s waste stream should be segregated to preserve recyclability.

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