| Код ТН ВЭД | 578613 |
Как аккредитованная фабрика ecovio IA1652 минерально наполненной компостируемой ПЛА для литья под впрыском, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
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Under the dual compostability frameworks applied to single-use cutlery, a finished fork or spoon must satisfy EN 13432:2000/AC:2005 or ASTM D6400-19, with the complete evidence chain centered on ISO 14855-1:2012 for ultimate aerobic biodegradation, ISO 16929:2013 or equivalent pilot-scale disintegration, and OECD 208:2006 ecotoxicity testing using compost contact. Food-contact status is assessed separately under Regulation (EC) No 1935/2004 and Commission Regulation (EU) No 10/2011 as amended by (EU) 2020/1245, with migration testing for aqueous, acidic, and fatty simulants drawn from EN 1186-1:2002. At the press, IA1652 is charged at 95–100 wt% with a 0–5 wt% EN 13432-compliant masterbatch fraction; external release-agent addition is held below 0.3 wt% because the mineral filler already reduces mold sticking and higher lubricant loadings produce vent-channel plate-out and subsequent gas-burn defects. The molding process for a 16-cavity cutlery tool on a 1600–2500 kN hydraulic toggle press operates with barrel temperatures at 190–210°C, nozzle temperature at 195–205°C, and mold coolant at 30–50°C; injection velocity is controlled to 180–250 mm/s, fill time is 0.6–1.1 s, and holding pressure is 700–1100 bar on the charge. Screw configuration with 20:1–22:1 L/D and 2.5:1–3.0:1 compression ratio is preferred because the mineral filler contributes abrasive viscosity and shortens material residence at elevated temperature. Gate blush appears when linear velocity exceeds 250 mm/s; splay, silver streaks, and reduced notched impact correlate with residual moisture above 250 ppm. Terminal article types are forks, knives, spoons, sporks, stirrers, and airline meal utensils that do not require post-crystallization to achieve serviceable rigidity.
When a coffee pod is injection-molded from IA1652, the processing conflict is the contrast between the 0.6–1.0 mm shell wall required for rapid disintegration in an industrial composting heap and the melt-pressure requirement imposed by a gate land near 0.4 mm. The mineral filler shortens spiral flow length relative to unfilled injection-molding PLA, so the converter must not transfer an unfilled-PLA gate position without flow-path correction; published spiral-flow data for this specific configuration is limited, and converter trials with a 0.8 mm shell-wall prototype are recommended before cutting steel. Certification for the pod is normally based on EN 13432:2000/AC:2005, with ISO 14855-1:2012 and ISO 16929:2013 used for the biodegradation and disintegration modules, and Commission Regulation (EU) No 10/2011 applied to the coffee-contact surface. The feed fraction at the press is 90–100 wt% virgin IA1652 with 0–10 wt% dry internal regrind from runners and rejected pods; masterbatch is added at 2–4 wt% because higher masterbatch loadings depress melt strength in thin sections. Accumulator-assisted electric-toggle molding machines are used to achieve injection velocities of 200–350 mm/s, fill times of 0.2–0.5 s, and holding pressures of 800–1200 bar; barrel set points are 190–215°C, the hot runner is maintained at 200–220°C, and total residence time above 200°C is capped below 5 min to prevent lactide volatilization and yellowing. The mold coolant is held at 20–45°C, and the operational boundary is explicit: the grade is not rated for continuous exposure to pressurized steam above 100°C; hot-extraction pods are limited to contact times under 30 s at delivered water temperatures below 95°C. Terminal products are single-serve beverage pods, tea pods, and portioned soluble-beverage cups where the wall must remain rigid during storage but still disintegrate after certification-grade composting.
For molded cosmetic jars, compact housings, and cap shells, the dominant failure mode is weld-line embrittlement where melt fronts recombine around a core pin or at a single edge gate. The required compliance envelope is EN 13432:2000/AC:2005 for compostability, Directive 94/62/EC for packaging and packaging waste, and REACH Annex XVII for restricted substances in the supplied article; cosmetic-formulation interaction testing is governed by Regulation (EC) No 1223/2009 for the cosmetic product, but the package is evaluated for migration under the same stability-protocol framework. The compound fraction is 70–90 wt% IA1652 blended with 10–30 wt% unfilled biodegradable polyester to raise deformation-to-break and reduce lid-to-jar crack propagation; loadings above 30 wt% flexible phase reduce thread-creep resistance below the threshold needed for repeated opening torque. Production uses a double-gated base feed with sequential valve-gate opening, 190–210°C melt temperature, 25–40°C mold temperature, and holding pressure of 600–900 bar; high-gloss cavity surfaces require steel finish below 0.05 µm Ra, and cooling time for a 25 mL jar wall is typically 12–18 s. Terminal article types are 15–100 mL cream jars, compact housings, twist-off caps, and collar closures in which the mineral-filled phase supplies opacity, scratch resistance, and lower shrinkage than unfilled PLA.
Toy components molded from IA1652 are evaluated under Directive 2009/48/EC, EN 71-1:2014+A1:2018 for mechanical and physical safety, and EN 71-3:2019+A1:2021 for migration of elements, while compostability claims follow EN 13432. The formulation is run at 100 wt% compound with 2–5 wt% EN 71-3-compliant masterbatch; internal sprue regrind is capped at 15 wt% after drying to residual moisture below 250 ppm. Molding is performed on vented multi-cavity tools with polished gate lands, melt temperature 190–215°C, mold temperature 25–35°C, and cycle time 15–25 s. Terminal parts are building blocks, board-game tokens, toy vehicle wheels, and figurine bases, where wall sections are maintained below 3.0 mm and living hinges are avoided because the mineral-filled grade has notched impact behavior that is inferior to unfilled PLA.
Because writing instrument housings require dimensional stability at wall cross-sections of 0.9–1.5 mm, the mineral-filled grade is used for pen barrels and desk accessories where warpage after molding is a measurable rejection cause. Compliance obligations are REACH Annex XVII and, for school stationery marketed to children, EN 71-1:2014+A1:2018 and EN 71-3:2019+A1:2021. The compound is metered at 80–100 wt% IA1652 with 0–20 wt% pre-dried internal regrind; a color masterbatch is added at 1–3 wt%. Production uses insert molding for metal pen nibs or clip springs on a 600–1200 kN press, barrel set points 190–215°C, mold temperature 20–35°C, injection velocity 200–300 mm/s, and holding pressure 700–950 bar. Terminal article types are pen barrels, rule housings, correction-tape bodies, desk organizer trays, and collapsible display stands.
Horticultural clips and plant fasteners are a misuse-prone segment because EN 13432 certification is tied to industrial composting conditions at 58°C and controlled humidity, not ambient soil burial. Soil degradation is assessed under ISO 17556:2019; without a published soil-biodegradation rate for IA1652, no claim should be made that a discarded clip will disintegrate in field soil. The molding formula is 100 wt% IA1652 with 0–2 wt% processing aid, and no aromatic UV stabilizer is added because outdoor exposure causes surface chalking after 10–12 months, which is conveyed as a one-season service limit. Processing uses single- and four-cavity tools with melt temperature 190–205°C, mold temperature 25–40°C, and injection velocity below 250 mm/s to prevent shear heating in thin hinge ribs. Terminal parts are nursery clips, vine ties, plant labels, seeding tray clips, and non-load-bearing tree guards.
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BASF ecovio® IA1652 is a mineral-filled injection molding grade identified by the supplier as a compostable PLA-based compound. The formulation is intended for rigid molded articles in which stiffness, dimensional reproducibility, and industrial compostability under EN 13432 are simultaneous requirements. The mineral phase functions as a reinforcing filler, raising elastic modulus and reducing post-mold shrinkage anisotropy relative to unfilled PLA. The product is supplied in pellet form and is applied principally in rigid packaging components, writing instruments, horticultural clips, coffee capsules, cosmetic packaging, and other thick- or thin-wall injection molded goods where compostability is needed at end of life.
Compounding of the mineral filler into the PLA matrix is typically performed on twin-screw extruders with L/D ratios above 32:1. Production experience shows that poor side-feeder calibration can generate filler agglomerates that appear later as surface pitting in molded parts. Melt-pressure fluctuation across the screen pack exceeding 1 MPa during compounding often correlates with dispersion instability or filler buildup on the screen. The compound is shear-thinning in the injection molding shear-rate range, and molders should not treat the ISO melt-flow value as a substitute for injection rheology.
The filler raises stiffness and lowers ductility when compared with unfilled PLA injection grades. Tensile modulus is evaluated according to ISO 527-2, and published datasheet ranges for this mineral-filled class typically fall between 3000 MPa and 4000 MPa. Tensile stress at break under the same method is generally in the range of 30 MPa to 45 MPa, with nominal tensile strain at break below 5%. Flexural modulus measured under ISO 178 usually exceeds the tensile modulus by a small margin because of the bending stress gradient. Notched Charpy impact strength under ISO 179-1/1eA at 23 °C is commonly below 5 kJ/m², indicating that the material is not suitable for impact-dominated snap-fit designs without careful gate location and wall-thickness analysis.
Heat deflection temperature under ISO 75-2/B at 0.45 MPa is a more meaningful thermal index for rigid packaging than Vicat softening temperature for this compound. Published datasheet ranges for heat deflection temperature are typically between 70 °C and 90 °C. Vicat A softening temperature under ISO 306 is often reported near 80 °C to 100 °C. These values are not load-bearing service temperatures; they are laboratory ranking metrics. For coffee capsule lids or bowls that contact hot food, the molder must verify dimensional stability under the actual load, contact time, and lip geometry.
Density is affected by the mineral filler and is measured under ISO 1183-1. Representative values for this grade class are in the range of 1.42 g/cm³ to 1.48 g/cm³. The higher density compared with unfilled PLA is a direct result of the mineral phase and must be included in per-part weight, packaging, and transportation calculations. Melt volume rate under ISO 1133-1 at 190 °C and 2.16 kg is typically in the range of 9 cm³/10 min to 15 cm³/10 min. This range supports injection molding flow lengths but does not describe the low-moisture viscosity response of the melt.
| Property | Standard method | Published range |
|---|---|---|
| Density | ISO 1183-1 | 1.42–1.48 g/cm³ |
| Melt volume rate | ISO 1133-1, 190 °C/2.16 kg | 9–15 cm³/10 min |
| Tensile modulus | ISO 527-2 | 3000–4000 MPa |
| Tensile stress at break | ISO 527-2 | 30–45 MPa |
| Nominal tensile strain at break | ISO 527-2 | 2–5% |
| Flexural modulus | ISO 178 | 3200–4200 MPa |
| Charpy notched impact strength, 23 °C | ISO 179-1/1eA | 2.5–5 kJ/m² |
| Heat deflection temperature, 0.45 MPa | ISO 75-2/B | 70–90 °C |
| Vicat A softening temperature | ISO 306 | 80–100 °C |
Moisture control, rather than barrel temperature, is the primary processing boundary for this compound. Pellets subjected to humid storage or open silo transfers absorb surface moisture, and PLA ester linkages undergo autocatalytic hydrolysis at melt temperature. A desiccant dryer is required when ambient relative humidity exceeds 60%. Pre-drying at 80 °C for 4 h to a residual moisture level below 0.025% by ISO 15512 is the standard starting condition. Hopper dryers without desiccant capability are not acceptable during high-humidity campaigns because the dew point cannot be held low enough. Moisture levels above 0.05% can produce visible splay, reduced melt viscosity, and loss of surface definition, particularly in multi-cavity tools with long melt paths.
Barrel temperature settings are typically profiled from feed to nozzle as 170–180 °C, 190–200 °C, 200–210 °C, and 200–210 °C. Melt temperature should be maintained between 190 °C and 210 °C. Short excursions to 220 °C may be acceptable only when the total residence time at that temperature is below 90 seconds. Sustained operation above 220 °C accelerates thermal chain scission and produces resin yellowing, reduced mechanical properties, and higher monomer outgassing. Screw recovery should be set so that total shot residence time at melt temperature remains below 8 minutes. During interruptions, the barrel should be purged with a PLA-based purging compound; polyolefin purge materials are not appropriate because they create contamination layers that are difficult to remove from hot runners and valve gates.
Mold temperature is a compromise between cycle time and part performance. The compound can be molded with mold temperatures between 20 °C and 80 °C. For thin-wall articles below 1.2 mm, mold temperatures above 40 °C improve cavity filling and surface replication but can extend cycle time. For thick sections above 3 mm, lower mold temperatures reduce sink-mark development but may increase molded-in stress and warp. Multi-cavity tools with runner diameters between 2 mm and 3 mm require balanced melt delivery because the mineral-filled compound has a narrower processing window than unfilled PLA. Vent depth should be held between 0.01 mm and 0.02 mm to permit gas evacuation without flash. Clamp force estimates of 3–6 kN/cm² of projected area are used as starting points for rigid packaging tools, but this is a general injection molding estimate and not a supplier-rated limit.
The mineral filler produces mild abrasive wear on screws, barrels, check rings, and hot-runner tips. Screws with hardened flights and bimetallic barrels are specified when sustained annual production volumes exceed roughly 50 tonnes per line. Otherwise, wear is often first observed as check-ring leakage that increases fill variability from shot to shot. Hot-runner thermal uniformity is more important with this compound than with unfilled PLA because partially cooled mineral-filled material can produce gate-stringing or cold plug formation in sub-runners.
Shrinkage of the mineral-filled grade is lower and less anisotropic than unfilled PLA. Post-mold shrinkage is not zero, and geometry with abrupt wall-thickness transitions can still develop sink marks if packing pressure is insufficient. Packing pressure should be applied through the gate freeze point; published data for this specific configuration is limited, but standard practice is to maintain packing pressure until gate freeze by monitoring cavity pressure rather than by relying on a fixed timer.
Thin-wall applications such as capsule bodies, lids, writing instrument barrels, and cosmetic sleeves often run at mold temperatures between 20 °C and 40 °C to shorten cycle time. Under these conditions, the mineral-filled compound develops lower heat resistance than the datasheet value because crystallinity remains limited. The lower mold temperature may also raise flow-front hesitation behind ribs and bosses, increasing visible knit lines. Weld-line strength under ISO 527-2 can be lower than the unfilled PLA reference, especially when two flow fronts meet after passing around a core pin. If weld lines are load-bearing, the gate should be relocated or the wall section adjusted rather than relying solely on mold-temperature increase.
Thin-wall processing requires higher injection velocities to prevent premature gate freeze. Injection velocity should be profiled so that the melt front does not drop below the hesitation threshold in ribs or hinges. For parts with wall thicknesses below 1.0 mm, cavity-fill analysis should include the effect of filler orientation on melt viscosity. The mineral phase orients during shear, reducing effective viscosity in the flow direction but also reducing transverse mechanical strength. This anisotropic behavior is measurable under tensile testing of specimens cut in and across flow, but published data for this specific configuration is limited.
When replacing unfilled PLA in an existing tool, the mineral-filled grade may require lower injection pressure because of its higher density and different compressibility, but the filled material may freeze faster at the same mold temperature. Gate size should be revalidated. Small gates optimized for unfilled PLA can restrict flow and produce high shear heating, causing local degradation in the gate region. Gate diameters for multi-cavity rigid packaging are usually kept above 0.8 mm for thin-wall parts; smaller gates are possible only with validated short fill times and hot-runner thermal control.
For applications involving hot contents, such as coffee capsules, the molder should not select ecovio IA1652 solely on the basis of heat deflection temperature. The actual capsule rim, seal, and body geometry must be tested under hot-water or hot-fill conditions because stress relaxation and hydrolytic decomposition compete with thermal distortion. The supplier’s EN 13432 certification does not itself establish food-contact suitability. Users must obtain written confirmation for specific migration limits under Regulation (EU) No 10/2011 or 21 CFR 175.300 where applicable. Published data for this specific configuration is limited, so application-specific migration testing is required.
| Standard or regulation | Clause or method | Boundary condition |
|---|---|---|
| EN 13432 | Packaging recovery; industrial composting | Requires biodegradation of at least 90% relative to reference within 180 days, disintegration leaving no more than 10% residue on a 2 mm sieve, and ecotoxicity evaluation under OECD 208. |
| ASTM D6400-23 | Compostable plastics for industrial facilities | Equivalent US certification path; not automatically equivalent to home compostability. |
| ISO 14855-1 | Aerobic biodegradation under controlled composting | Used for biodegradation percentage evidence; certification documentation should be matched to the specific lot or grade. |
| ISO 20200 | Laboratory-scale disintegration | Residue fraction is measured after composting; passes only within the EN 13432 certification scope. |
| RoHS 2011/65/EU | Electrical and electronic equipment | Relevant only if the molded article falls under electrical/electronic scope; supplier declaration is required. |
| REACH SVHC | Candidate list | No regulatory assumption should be made without a current supplier statement. |
Published data for long-term storage of ecovio IA1652 at high ambient humidity is limited. The material should be stored in sealed packaging below 30 °C and re-dried after any exposure exceeding 30 minutes in ambient air before processing. The compound is not a home compostable product unless separately certified; the standard industrial composting certification does not automatically transfer to low-temperature backyard conditions. The material should also not be exposed to alkaline fillers or additives that shift hydrolysis equilibrium, because such changes can reduce compostability and molded-part service life. Processors should verify all critical parameters against the current manufacturer certificate of analysis rather than relying on class-typical ranges.