| Код ТН ВЭД | 501304 |
Как аккредитованная ETEC (EnvisionTEC) ETEC WIC 100 серии легкоутвердительной смолы фабрика, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
| Упаковка | ETEC WIC 100 Series light-curing resin supplied in a 1 kg opaque plastic bottle with screw cap and hazard labels. |
| Погрузка контейнера (20-футовый контейнер) | 20′ FCL container loading: palletized EnvisionTEC ETEC WIC 100 Series light-curing resin drums, labeled, secured, braced for safe ocean transport. |
| Доставка | ETEC WIC 100 Series light-curing resin is shipped in sealed, opaque, original containers, protected from UV light, heat, and freezing. Keep away from ignition sources. Consult the SDS for transport classification; may be non-regulated. If regulated, use the correct UN number, proper shipping name, hazard class, packing group, labels, and emergency documentation. |
| Хранение | Store ETEC WIC 100 Series light-curing resin in its original, tightly closed container in a cool, dry, well-ventilated area. Protect from direct sunlight, UV light, heat, sparks, and flames. Keep away from incompatible materials, moisture, and ignition sources. Maintain stable room temperature; do not freeze. Keep out of reach of children. Follow the SDS. |
| Срок годности | Shelf life is typically 12 months when stored unopened in the original container at 18–25°C, protected from light and heat. |
In precious-metal casting shops running centrifugal or vacuum induction casting units, the ETEC (EnvisionTEC) WIC 100 Series light curing resin functions as a direct lost-wax pattern material. The resin is a single-component photopolymer; no catalyst addition, solvent dilution, or filler adjustment is required before printing. Viscosity control is performed at 25 °C using a cone-plate viscometer according to ISO 2884-1:2006; when the certificate of analysis value falls outside the printer recoat envelope, build-to-build variation in green strength appears as fine-feature curl and support detachment. Patterns are built on DLP equipment operating at 405 nm, typically at layer thicknesses of 25 μm or 50 μm, with exposure energy adjusted for blackback or high-resolution print modes. Uncured resin removal uses water at 20–30 °C in an agitated bath or ultrasonic cleaning unit equipped with frequency settings from 35 kHz to 45 kHz; isopropanol is not required. Wash water must be replaced before turbidity exceeds the process-defined limit because dissolved monomer reduces wash efficiency; published data for the monomer saturation point of this resin in water is limited. After rinsing, components are air-dried and inspected for occlusion of fine filigree recesses. Spruing geometry follows investment casting practice: larger patterns require a reservoir or expansion bulb, and distal thin sections below 0.3 mm are reinforced because green photopolymer strength is anisotropic and may distort during rinsing. The printed pattern is mounted on a metal sprue base and vacuum-mixed with a gypsum-bonded investment; a typical powder-to-water ratio for jewelry flask investment is 100:28 to 100:32, but the exact ratio must be taken from the investment manufacturer’s datasheet. Vacuum mixing at 0.1 bar absolute and bench setting for 2 h reduce bubble entrapment on the pattern surface. Burnout is staged: a first ramp at 1–2 °C/min to 150 °C, a 60–90 min hold to drive off water, a second ramp at 1–1.5 °C/min to 730 °C, and a 3 h hold to mineralize carbon residues. The furnace must have oxygen ingress during resin decomposition; sealed or nitrogen-blanketed burnout profiles produce carbon-rich residues. After burnout, gold, platinum, or sterling silver alloys are cast at temperatures between 980 °C and 1020 °C for gold and approximately 1020–1100 °C for silver alloys, depending on alloy liquidus plus superheat. Final precious-metal articles—rings, pendants, bracelet links, and filigree settings—are inspected for gas porosity by radiography or ASTM E562 image analysis. Compliance of the resin itself is limited to occupational handling under REACH (EC 1907/2006) and disposal according to local photopolymer waste codes; EU nickel release compliance under EN 1811:2011+A1:2015 is an alloy property and not a resin property. Published data for WIC 100-specific ash residue after burnout is limited; foundries should verify residue below 0.05 wt% using a muffle furnace ashing test adapted from ISO 1172:1996 before committing to production.
Dental laboratories using lithium disilicate and leucite-reinforced glass-ceramic ingots evaluate WIC 100 Series resin as a substitute for hand-waxed or milled polymer patterns in the pressable ceramic process. The pattern resin is not used as a final intraoral material; it must disappear completely during the press furnace burnout cycle before the ceramic ingot is pressed into the void. Mixing ratio for the press investment is specified by the investment manufacturer, commonly near 100 g powder to 22–24 mL liquid for high-expansion formulations, but no additional ratio modifier is added to compensate for polymer degradation. Patterns are printed at 50 μm or 25 μm layer thickness, washed in water at 20–28 °C, dried under filtered air, and sprued with resin or wax sprues of sufficient length to create a press channel. In the pressing furnace, wax/resin elimination is performed at a final burnout temperature of 850 °C for 45–60 min for many pressable ceramic systems; lithium disilicate ingots are then pressed at 920–950 °C under vacuum. The risk is carbon retention if the burnout dwell is shortened because carbon at the marginal interface inhibits ceramic wetting and produces edge chipping. Press furnace loading is limited by the ingot mass for the restoration; for a molar crown, a 1.0 g ingot is common, while veneers and inlays may use 0.5 g ingots. Final restorations—pressable lithium disilicate crowns, inlays, onlays, and veneers—are finished with ceramic stains and glazed. Compliance of the fired ceramic is evaluated under ISO 6872:2015 and ISO 9693:2019 for metal-ceramic bond strength where applicable. The resin itself has no direct role in final biocompatibility, but a dental laboratory must document that no uncured monomer remains in the pore structure; this is checked by gas chromatography-mass spectrometry on sintered investment debris if full clearance is unknown. Published data for WIC 100-specific press furnace compatibility with pressable ceramic cycles is limited; a single-flask trial is used before full production.
Removable partial denture frameworks cast from cobalt-chromium alloys subject the pattern material to an environment that combines high pouring temperatures with phosphate-bonded investment chemistry. WIC 100 Series resin patterns are produced on DLP equipment and washed in water at 20–30 °C; residual moisture is removed in a convection dryer at 40–50 °C for at least 15 min because trapped water inside thin clasps can disrupt phosphate investment setting. Resin patterns are then attached to a refractory cast or castable pattern base using sticky wax or resin. The phosphate-bonded investment is mixed according to manufacturer ratio, typically 100 g powder to 20–24 mL colloidal silica liquid; the expansion properties depend on the liquid dilution. Mixing under vacuum at 450 rpm for 60 s and pouring under vibration prevent bubbles on occlusal rest seats and clasp tips. Burnout follows a staged cycle: drying at 150 °C, a controlled ramp of 1 °C/min between 150 °C and 600 °C, a hold at 900 °C for 2–3 h, and casting at 1450–1480 °C for cobalt-chromium alloys. The slow ramp through the polymer decomposition band reduces carbon residue and minimizes chromium carbide formation. Cast framework terminal products include lingual bars, circumferential clasps, rest seats, and mesh retention structures. Final alloy compliance is assessed under ISO 22674:2016 for metallic dental restorations and ISO 10993-5:2009 for cytotoxicity where the framework is placed in prolonged tissue contact. The pattern resin must be completely eliminated; if carbon residue exceeds 0.1 wt% as measured by combustion analysis of residual investment, the framework lot is rejected for visible porosity and possible carbide inclusions. Published data for WIC 100-specific behavior in phosphate-bonded investments is limited; each flask configuration requires one destructive qualification casting.
Small-lot precision foundries producing austenitic and precipitation-hardening stainless steel components use WIC 100 Series resin where pattern complexity exceeds wax tooling economics or where water-washable cleanup reduces solvent consumption. The resin is printed as a single-component pattern; no liquid-to-powder ratio exists at the pattern stage. Ceramic shell construction follows the same sequence used for wax patterns: a prime coat of zircon flour in colloidal silica, fused silica backup coats, and final seal coat. Each shell layer is dried at 23–25 °C and 45–60% RH; the pattern and shell remain compatible only if the first coat is applied within 2 h after water washing and drying. Burnout is performed in an air-ventilated furnace with a ramp from ambient to 180 °C at 1 °C/min, a 1 h dwell, then a ramp to 1050 °C at 2–3 °C/min, and a 2 h hold before casting. Austenitic 316L and martensitic 17-4 PH stainless steel alloys are poured at 1550–1600 °C and 1560–1620 °C respectively, depending on superheat and shell temperature. Terminal parts include micro-valve bodies, orthopaedic trial instrument handles, watch case components, and fluid connector parts. Final mechanical properties are defined by ASTM A240/A240M or ASTM A564/A564M depending on alloy, and passivation compliance is evaluated under ASTM A967/A967M. Resin removal is not a final-material compliance statement; if patient-contacting status applies, the finished metal must meet ISO 10993-1:2018 biocompatibility requirements. Published data for WIC 100-specific ceramic shell interaction in stainless steel investment casting is limited; a prime-coat wetting test and trial casting are required for each new shell slurry batch.
Orthodontic laboratories that cast custom clasps, band-and-loop space maintainers, and transpalatal arch frameworks use WIC 100 Series resin to replace wax hand-forming where repeatable wire-to-cast junction geometry is required. Printed patterns are generated at 25 μm layer thickness to capture bolt hole details and wire insertion slots. Water washing at 20–28 °C with a fine brush removes trapped uncured resin in socket areas; isopropanol is not required, which simplifies waste handling in a dental facility. Sprues are attached at right angles to the largest cross-section; for band loops, two 0.5–0.8 mm round sprues feed the loop to avoid cold shuts. Investment mixing ratios for orthodontic casting are the same as for removable partial denture frameworks—phosphate-bonded investment mixed at 100 g powder to 20–24 mL liquid—but flask size is smaller, and burnout time may be shortened after thermal profiling. A typical small-flask burnout uses a 150 °C drying hold, 1 °C/min ramp to 900 °C, and 2 h hold, followed by casting of nickel-free chromium-cobalt or commercially pure titanium alloys. Final devices—space maintainers, distal extensions, and transpalatal arches—are polished and passivated before intraoral delivery. Compliance is controlled under ISO 22674:2016 for the cast alloy and ISO 10271:2020 for corrosion resistance of metallic intraoral devices. The resin is a processing aid and is not present in the appliance; residual carbon in the cast surface is checked by scanning electron microscopy with energy-dispersive X-ray spectroscopy. Published data for WIC 100-specific performance with commercially pure titanium casting is limited; titanium’s high reactivity with carbon and oxygen requires a dedicated argon-arc casting unit and a resin burnout qualification coupon.
| Scope | Standard or method | Measured endpoint | Application-specific acceptance |
|---|---|---|---|
| Resin viscosity control | ISO 2884-1:2006 | Single-component resin at 25 °C | Certificate of analysis value within printer recoating envelope |
| Ash residue after burnout | Ashing adapted from ISO 1172:1996 | Inorganic residue | <0.05 wt% for precious metal casting; <0.1 wt% for Co-Cr frameworks depending on alloy |
| Final metal porosity | ASTM E562 | Area fraction porosity at polished cross-section | <2% for structural components |
| Nickel release from final article | EN 1811:2011+A1:2015 | Nickel ion release | <0.5 μg/cm²/week for prolonged skin contact; <0.2 μg/cm²/week for piercing post assemblies |
| Dental metallic restoration requirements | ISO 22674:2016 | Mechanical and chemical properties | Alloy-specific proof stress, elongation, and corrosion resistance |
| Ceramic restoration requirements | ISO 6872:2015 | Flexural strength, chemical solubility | Class-specific minima for pressed ceramic |
| EU chemical regulation | REACH (EC 1907/2006) | SVHC content and safe-use communication | Verify WIC 100 Series safety data sheet and supplier declaration |
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ETEC WIC 100 Series is a liquid methacrylate-based photopolymer supplied by ETEC (EnvisionTEC) for vat photopolymerization platforms operating in the 385–405 nm band. The resin is formulated as a water-clear impact grade, meaning that the cured polymer retains translucency while providing a higher elongation-at-break envelope than conventional rigid clear acrylates. The product is used on digital light processing (DLP), scan-spin-selectively photocure (3SP), and continuous digital light manufacturing (cDLM) systems equipped with compatible UV-A projectors. Manufacturer documentation classifies WIC 100 as a prototyping and indirect manufacturing resin, not as a burnout casting resin, biocompatible dental resin, or high-temperature tooling resin. Incoming resin is controlled by lot, and certificates of analysis report liquid density, dynamic viscosity, and photoactive solids content. Cured-property qualification is commonly performed using ASTM D638 for tensile response, ASTM D790 for flexural modulus, ASTM D2240 for Shore D hardness, ASTM D648 for heat deflection temperature, and ASTM D570 for water absorption. Optical acceptance of polished parts is expressed through ISO 13468 total luminous transmittance and ASTM E313 yellowness index.
In the ETEC resin portfolio, WIC 100 occupies a different position from PIC 100-class sacrificial casting resins, E-Model Light opaque ABS-like grades, and HTM 140 high-temperature tooling resins. The principal difference is the combination of optical clarity and impact-oriented failure strain. Technical bulletins classify WIC 100 as a water-clear impact prototype material rather than a burnout material for precious-metal casting. Investment foundries generally specify PIC-series resins because those grades are formulated for clean burnout and lower residual ash; WIC 100 is not marketed with an ash content specification for direct casting. Compared with opaque ABS-like modelling resins, WIC 100 enables inspection of internal channels, fluid paths, or light-guide geometry without destructive sectioning. Compared with high-temperature mold resins, WIC 100 has a lower service ceiling and is not rated for short-run injection tooling. The distinction is also visible in post-processing: clear parts require surface polishing or clear coating to reduce layer-line haze, whereas opaque engineering grades are often tested in the as-built or lightly sanded state.
For preliminary design work, the following material-class envelope is used. Lot-specific values from the WIC 100 certificate of analysis take precedence over these broad class limits.
| Property | Test method | Unit | Material-class envelope |
|---|---|---|---|
| Liquid viscosity at 25 °C | ISO 3219 / ASTM D7867 | mPa·s | 700–1,200 |
| Tensile strength at break | ASTM D638 | MPa | 35–55 |
| Elongation at break | ASTM D638 | % | 15–30 |
| Flexural modulus | ASTM D790 | GPa | 1.0–2.5 |
| Shore D hardness | ASTM D2240 | — | 70–85 |
| Heat deflection temperature at 0.45 MPa | ASTM D648 | °C | 55–80 |
| Water absorption after 24 h | ASTM D570 | % | 0.5–1.5 |
On 3SP and cDLM platforms, the practical processing window is controlled more by vat temperature and resin viscosity than by projector irradiance alone. Green-part quality declines when the liquid is colder than 20 °C because the material does not recoat uniformly over large solid cross-sections. The standard preparation procedure is to roll the container for 30 min and equilibrate the vat to 23 ± 2 °C before starting a build. If viscosity measured according to ASTM D7867 exceeds the upper limit in the table, the resin may be outside its intended recoat envelope for standard DLP or 3SP dynamics. The resin should not be diluted with water or isopropanol; polar contaminants disrupt free-radical polymerization and create tacky surfaces. Resin age, ambient humidity, and long exposure to low-intensity stray light alter the photoactive species, so an all-window exposure test is performed after any material change.
On an ETEC 3SP platform such as the Xtreme 8K with a 405 nm LED projector, WIC 100 is generally run at 50–100 µm vertical slice thickness. The exposure per layer is programmed as a dose integral, not a single time, because large-area solid sections require different irradiance compensation than isolated supports. On cDLM systems with an oxygen-permeable build interface, the dead-zone thickness changes with irradiance, resin viscosity, and part cross-section; WIC 100 typically requires lower continuous pull speed than low-viscosity dental resins to prevent delamination of large cross-sections. The build engine records projector power, exposure time, and temperature; these records are required for lot traceability and troubleshooting. Published data for this specific configuration is limited, so new installations should be qualified with a standardized build containing vertical and horizontal ASTM D638 specimens, a 50 mm diameter disk, and a sectioned hollow channel.
Mechanical performance in photopolymer parts is anisotropic because the weakest plane often lies between successive layers. In WIC 100 builds, the difference between xy-plane tensile elongation and z-axis tensile elongation can be the controlling factor for load-bearing prototypes. One practical evaluation method is to machine slabs from a 10 mm-thick build block and extract tensile bars parallel and perpendicular to the build direction, then test according to ASTM D638. If z-axis elongation falls below 70% of the xy-plane value, thin vertical walls under snap deflection may require design changes or alternative orientation. Post-curing in a 405 nm chamber at moderate temperature increases crosslink density and surface hardness but also increases brittleness; the post-cure cycle is therefore balanced against the required impact performance. Fourier-transform infrared analysis of the carbonyl or acrylate peaks is used for process control when changing post-cure lamps or layer thickness. Published data for this specific configuration is limited, so acceptance limits are generated from internal build qualifications.
Transparent fluid-flow visualization manifolds are built in WIC 100 because the cured polymer permits internal inspection without destructive sectioning. Luminous transmittance acceptance is often linked to ISO 13468, and yellowness index to ASTM E313. Polishing with 600–1200 grit abrasives followed by a clear acrylic lacquer is used to reduce layer-line scattering. For impact-loaded snap-fit or housing prototypes, design practice requires both xy-plane and z-axis test specimens because photopolymer layer interfaces produce anisotropic tensile elongation. Notched Izod impact according to ASTM D256 is measured before risk-prone features are placed near the build platform. The resin is also used for short-run transparent covers, lens prototypes, and packaging display parts in which the user evaluates form, fit, and visual appearance rather than production-grade optical performance.
Common production-line failure modes observed with water-clear impact resins include vat film clouding, part chipping during support removal, and surface crazing after excessive solvent exposure. Vat film clouding occurs when polymerized debris remains on the release surface or when ambient dust enters the vat. Parts left in solvent immersion exceeding 5 min can develop microcracks, especially around sharp corners or thick-to-thin transitions. Support removal is therefore performed before solvent immersion where possible, using sharp diagonal cutters with the part at room temperature. If chilled, the material becomes more brittle and the probability of chipping at support contact points increases. Surface crazing is evaluated under 20× magnification after solvent immersion; any visible microcrack network is recorded as a process deviation.
Cured WIC 100 is not specified for continuous service in pressurized aqueous lines or repeated steam sterilization. Water absorption measured according to ASTM D570 gradually reduces the glass-transition-related performance, and wetted parts may show a measurable reduction in ASTM D790 flexural modulus and ASTM D648 heat deflection temperature. Chemical compatibility should be examined with the actual process fluid because aromatic hydrocarbons, ketones, and strong alkaline cleaning agents can attack the crosslinked acrylate network. Compatibility testing follows ASTM D543; the part is immersed for a defined period and then re-measured for hardness, mass change, and visual surface degradation. Outdoor exposure increases ASTM E313 yellowness index over accumulated UV-A dose, even when a UV stabilizer package is present in the formulation. Optical prototypes intended for prolonged natural light should therefore be used as short-term evaluation aids rather than as permanent glazing components.
Uncured resin handling follows standard photopolymer safety procedures. The material is classified as a skin and eye irritant; operators wear nitrile gloves and sealed eye protection during vat filling, filtering, and part removal. Spent wash solvent contains uncured monomer and should be disposed of as hazardous liquid waste. Internal channels and blind holes can retain uncured resin after bulk washing; they are flushed with ≥99% isopropanol and exposed to a 405 nm light guide before the part is considered safe for routine handling. The manufacturer’s safety data sheet and lot-specific certificate of analysis are the controlling documents for regulatory, storage, and disposal requirements. Standard resin shelf life is stated on the container label; expired material should not be blended into fresh vat stock because photoinitiator depletion produces under-cured surfaces and powder deposits on the vat film.