| Код ТН ВЭД | 680989 |
Как аккредитованный завод по производству смолы для высокотемпературной 3D-печати Henkel Loctite 3D IND147™ HDT230, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
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Under-hood connector housings and sensor brackets are built from Henkel Loctite 3D IND147™ HDT230 high-temperature 3D printing resin for short-loop design verification before injection-moulded polyamide or PPS tooling is released. The build file uses 100 % solid infill, 50 µm layer thickness, and a platform temperature from 25 °C to 35 °C. Support contact diameter is set to 0.3 mm to reduce scar-induced stress concentration. Green parts are washed in isopropanol or a Henkel-qualified solvent. Solvent immersion time is limited to the supplier’s published cleaning instruction. Post-cure is performed in a 405 nm LED flood chamber followed by a manufacturer-specified thermal hold. The terminal part is an engine-bay sensor bracket or connector latch that must withstand 150 °C continuous dry heat for 1000 h without crack formation or latch force loss. Test methods include ISO 527-2:2012 for tensile modulus retention, ISO 178:2019 for flexural modulus, and ISO 16750-4:2023 for thermal cycling from −40 °C to 150 °C. Dimensional inspection is performed on a calibrated coordinate measuring machine after each cycle block.
Process control is dominated by residual monomer content after post-cure. Incompletely post-cured parts show reduced modulus at 150 °C. The post-cure chamber must provide uniform irradiance over the entire build envelope. Hot spots above 60 °C during post-cure can cause thermal warping of thin flanges. Printed flanges are fixtured flat during the thermal hold. On short-run production lines, the principal failure mode is support removal tearing at the layer interface. This is controlled by orienting the part at 45° to the recoater blade and placing supports on non-mating surfaces. For under-hood approval, RoHS 2011/65/EU and REACH Regulation (EC) No 1907/2006 SVHC declarations are included in the customer submission. Published data for this specific resin and automotive test configuration is limited; each new geometry must be qualified on the targeted DLP platform.
Lead-free wave solder pallet carriers printed from IND147 operate at the upper thermal boundary of the resin. Peak contact temperature is normally 260 °C to 270 °C for 3 s to 5 s per pass. A solid flat plate warps after the first pass because the top surface expands more quickly than the lower surface. Rib geometry reduces oil-canning and permits forced-air cooling between passes. The build file uses a 3 mm top skin, 5 mm tall ribs, and rib spacing not larger than 40 mm. Rib axes are oriented at 45° to the recoater blade. Solid infill is used under PCB support pads. The remaining volume uses 25 % triangular sparse infill. Post-cure uses 405 nm irradiation and a thermal ramp not exceeding 1 °C/min to limit residual stress. The finished pallet carrier is qualified by thermal shock testing to IEC 60068-2-14:2009 for 50 cycles between 30 °C and 230 °C. Warpage is measured on a granite surface plate with a 0.05 mm dial indicator. Compliance for lead-free processing is evaluated under RoHS 2011/65/EU and IPC-A-610 visual cleanliness criteria. Tin-lead compatibility is not automatic; flux residues from high-tin alloys may interact with the polymer surface.
Flux exposure is a critical process limit. Rosin-free acidic fluxes with pH below 4.0 can etch the surface. A wipe with isopropanol after every shift removes flux accumulation. Automated cleaning lines that use ultrasonic baths should not be adopted without supplier qualification. Cavitation can propagate microcracks along layer planes. Printed pallets are stored flat at 23 °C ±2 °C and 50 % ±10 % relative humidity. Bowing after storage is controlled by reverse fixturing during post-cure. First-article inspection includes cross-section microscopy for delamination and dye penetrant inspection according to ASTM E1417-21. Published data for this specific configuration is limited. A qualification report must include thermal shock results, dimensional change, and surface hardness retention.
| Application | Primary standard | Test method / condition | Controlled parameter |
|---|---|---|---|
| Under-hood sensor bracket | ISO 16750-4:2023 | Temperature cycling −40 °C to 150 °C | Crack formation, latch force |
| Lead-free solder pallet | IEC 60068-2-14:2009 | Thermal shock 30 °C to 230 °C, 50 cycles | Warpage, delamination |
| Autoclave layup tool | ISO 294-4:2018 | Linear shrinkage after autoclave cycle | Tool flatness, seal plane |
| Injection mould insert | ISO 294-3:2020 | Shrinkage measurement after 150 shots | Dimensional drift |
| Geothermal sensor shroud | ISO 62:2008 | Immersion in simulated brine 180 °C, 168 h | Swelling, microcracking |
| Burn-in socket plate | IEC 60243-1:2013 | Dielectric strength at 150 °C | Insulation resistance |
For autoclave tooling of small-batch carbon fibre epoxy prepreg components, a printed photopolymer master is used only for female layup shells. The tool is printed with 100 % solid polymer and 20 µm z-resolution to maintain surface profile. The layup face is coated with a release system compatible with Henkel cleaning solvents. During autoclave cure at 180 °C and 0.7 MPa, the bulk polymer temperature is below the published HDT of 230 °C at 0.455 MPa according to ISO 75-2:2013 Method B. The pressure condition is more severe than the HDT test condition. Unsupported tool spans are therefore limited to 150 mm. Aluminium backing ribs are bolted to the printed shell through preformed holes. Flatness is checked before and after each cycle according to ISO 1101:2017. Linear shrinkage is measured according to ISO 294-4:2018. The terminal product is a female layup tool used for 20 to 50 autoclave cycles. Compliance documentation includes REACH Regulation (EC) No 1907/2006 and RoHS 2011/65/EU. Published data for long-term autoclave ageing of this specific resin is limited.
Short-run polyamide 66 injection trials use IND147 for cavity inserts in steel mould bases. The insert is printed solid with 100 % infill and post-cured to full crosslink density. The gate region and ejector system remain steel because molten PA66 at 285 °C to 300 °C and injection pressure from 80 MPa to 120 MPa exceed the load capacity of the photopolymer. Cooling is provided by a steel backing plate with water lines at 60 °C. A mould-open cooling pause of 10 s to 20 s is inserted before ejection to reduce heat accumulation. Cavity wall thickness is kept below 8 mm to limit thermal mass. The insert is used for 150 shots of glass-fibre-reinforced PA66 connector bodies. Shrinkage is recorded according to ISO 294-3:2020. Surface cracking and gas trapping are inspected after every 25 shots. Published data for this specific configuration is limited. The resin insert is a bridge tool for design verification and low-volume assembly trials, not a replacement for tool steel in high-volume production.
Ejection force is a failure driver. Draft angle on the printed cavity is set to 2° minimum. The polymer surface has lower thermal conductivity than steel, so cycle time is longer. Hot spots occur adjacent to the gate. If the gate is incorrectly positioned, local surface degradation appears as white blistering. Process engineers record insert temperature with a contact thermocouple after ejection. If surface temperature exceeds 230 °C, cooling pause is extended. Dimensional drift after 150 shots is compared against first-shot cavity dimensions. Published data for this specific configuration is limited.
Geothermal downhole tool prototypes use IND147 for sensor shrouds around metal electronics housings. The shroud is a dielectric spacer, not a pressure boundary. The part is printed with 50 µm layers, 100 % infill, and radial orientation to place layer planes perpendicular to hoop stress. Continuous immersion testing in simulated brine at 180 °C with 50 ppm H2S is performed for 168 h. Dimensional swelling is measured according to ISO 62:2008. The polymer is not listed in NACE MR0175/ISO 15156:2015; therefore, sour gas pressure is isolated by a stainless steel sleeve. The terminal shroud is used in wireline evaluation tools for 8 h to 12 h runs. Microcrack detection after retrieval uses dye penetrant according to ASTM E1417-21. Compliance documentation includes supplier SDS and GHS classification for transport. Published data for long-term hydrolysis of this specific resin at geothermal conditions is limited.
Thermal expansion mismatch between the polymer shroud and stainless steel housing is compensated by a sliding fit with 0.1 mm radial clearance. The clearance is calculated from coefficient of linear thermal expansion measurements. If the clearance is too tight, hoop stress at 180 °C causes axial cracking. If too loose, vibration during wireline descent produces fretting dust. Surface finish is measured with a stylus profilometer at Ra 3.2 µm. Post-cure residual stress is reduced by a controlled thermal ramp. Independent data for this specific resin under sour brine ageing are limited.
Printed socket mounting plates locate contact pins and thermocouples in semiconductor burn-in fixtures. The photopolymer replaces machined PEEK or polyimide for low-volume test hardware where lead time and internal feature complexity are constrained. Feature-to-feature positional tolerance is held at ±0.1 mm through exposure calibration on the target DLP machine. Build orientation places pin holes parallel to the Z-axis to maintain roundness. The plate is post-cured, then dry-heated at 150 °C for 4 h to remove residual monomer. Dielectric strength is measured according to IEC 60243-1:2013. The assembly is operated intermittently at 175 °C for 1000 h. Pin insertion force is checked after every 250 h interval. Compliance for electrical safety is assessed under IEC 61010-1:2010/AMD1:2016. The terminal component is a burn-in socket carrier for 0.5 mm pitch test sockets. Published data for this specific configuration is limited. High-voltage pins above 48 V require independent validation because the resin has no certified electrical insulation grade.
Pin hole roundness is measured on a vision measuring machine with 0.005 mm resolution. Hole wall roughness after printing is reduced by selecting 20 µm layer thickness. The plate is conditioned at 23 °C ±2 °C and 50 % ±5 % relative humidity for 24 h before dimensional inspection. Dielectric testing at elevated temperature must include a pre-test thermal soak to stabilise the polymer. Surface contamination from release film residues increases leakage current. The plate is cleaned with isopropanol and blown dry with filtered air before electrical test. Published data for this specific resin under high-temperature electrical stress are limited.
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Henkel Loctite 3D IND147™ HDT230 High-temperature 3D printing resin is a single-component, UV-active photopolymer supplied for digital light processing equipment operating at 385 nm to 405 nm. The suffix HDT230 identifies the manufacturer-reported heat deflection temperature of 230 °C at 0.455 MPa after the complete post-cure protocol, measured according to ASTM D648 / ISO 75-2 Method B. The uncured material is a dark, rigid photopolymer with a dynamic viscosity at 25 °C reported by ISO 2884 in the 300–500 mPa·s range. That viscosity permits recoating in most 4K and higher-resolution DLP platforms without heated vat modification, provided the build room is maintained above 20 °C. The resin is intended for rigid high-temperature tooling, conformal cooling inserts, short-run mold components, and underhood test fixtures. It is not formulated for material extrusion, fused filament fabrication, or highly flexible impact-loaded parts. General-purpose DLP resins commonly report heat deflection temperatures below 60 °C at 0.455 MPa; this product shifts the application envelope toward elevated-temperature tooling at the expense of elongation at break, which is reported near 1–2% per ISO 527-2. The resin is supplied as an industrial photopolymer, not as a consumer adhesive.
The uncured resin is commonly available in 1 kg containers for industrial evaluation. Because the photoinitiator package responds to 385 nm and 405 nm, the material can be used on LED-DLP and laser-based stereolithography platforms with appropriate resin handling modifications. However, mechanical property data should not be assumed to transfer across machine types without revalidation. Open-architecture DLP printers with metal-backed build plates and recoat blades are the primary intended equipment. Build parameters such as exposure time, wait time, and recoater speed must be calibrated on the target machine because dark resins absorb and scatter UV differently than clear or translucent photopolymers.
Heat deflection temperature is not a maximum continuous service temperature. The 0.455 MPa HDT result describes the temperature at which a standard test coupon deflects 0.25 mm under three-point bending at a defined heating rate. For Loctite 3D IND147 HDT230, the 230 °C result is a short-term comparative thermal index, not a guarantee of dimensional stability under asymmetric clamp loads, thermal gradients, or long-term creep. In a clamped tool insert or sealing surface, local stress routinely exceeds 0.455 MPa; the usable ceiling is therefore lower than 230 °C unless part-level qualification demonstrates adequate creep resistance. The public technical datasheet does not provide a full creep-rupture envelope for this product, so long-term load-bearing applications above 150 °C require creep testing according to ASTM D2990 or ISO 899-2. Published data for sustained creep under humid conditions above 100 °C are limited, and industrial users should not extrapolate the HDT value to continuous stress at 0.5 MPa or greater.
On a production DLP cell using an 8.9-inch 4K projector and a metal-backed build plate, build failures in high-temperature resins of this class are often linked to resin temperature rather than exposure dose. When the vat temperature drops below 20 °C, viscosity increases and thin walls below 2 mm may exhibit edge lifting at the z-interface. The control is to maintain resin temperature at 25–35 °C and to program a short post-exposure delay of 1–3 s for narrow negative features. Layer thickness is typically 50 µm or 100 µm; finer layers improve vertical resolution but increase interlayer interface count and total build time. Green parts are brittle and must be cleaned with the manufacturer-approved solvent. Residual solvent trapped in blind holes can plasticize the partially cured surface and reduce final hardness. After cleaning, a two-stage post-cure is required. A UV-only post-cure at ambient temperature does not yield the 230 °C HDT, and the thermal stage specified in the manufacturer’s technical datasheet must be followed exactly. Large unsupported planes can warp if the thermal ramp is too fast after UV exposure; support placement and build orientation should be designed to reduce restraint during shrinkage.
The following values are representative lot-average data drawn from the manufacturer’s published technical literature for fully post-cured specimens. They are not batch-specific specification limits. Where a range is shown, the value accounts for variation across published revisions and test-laboratory reports; a current certificate of analysis should be requested for production lots used in tooling applications.
| Property | Test method | Reported typical value |
|---|---|---|
| Heat deflection temperature at 0.455 MPa | ASTM D648 / ISO 75-2 Method B | 230 °C |
| Tensile strength at break | ISO 527-2 | 40–60 MPa |
| Tensile modulus | ISO 527-2 | 2.5–4.0 GPa |
| Elongation at break | ISO 527-2 | 1–2% |
| Flexural strength | ISO 178 | 60–90 MPa |
| Flexural modulus | ISO 178 | 2.5–4.0 GPa |
| Hardness | ISO 868 / ASTM D2240 | 85–90 Shore D |
| Dynamic viscosity at 25 °C | ISO 2884 | 300–500 mPa·s |
| Cured density | ISO 1183-1 | 1.15–1.25 g/cm³ |
The low elongation and high hardness indicate a brittle, highly crosslinked glassy network. This property set supports short-term elevated-temperature stiffness but makes the material sensitive to sharp internal corners and stress concentrations. Flexural strength values reported for photopolymers are often orientation-dependent; users should test flat and on-edge specimens per ISO 178 and establish internal acceptance limits from a minimum of three build jobs per ISO 17296-2.
The apparent viscosity of high-temperature DLP resins is shear-thinning at the recoater blade; therefore, measuring viscosity with a cone-and-plate viscometer per ISO 2884 does not fully predict recoat behavior. On equipment with a recoater blade gap of 100–200 µm, the material should be allowed to reflow until the liquid surface is flat before exposure. For a 50 µm layer, dynamic reflow times in unheated vats can be 2–5 s depending on resin temperature and blade speed. In multi-part builds with sparse packing, edge meniscus effects are reduced by increasing wait time rather than increasing light dose. High light dose in dark resins can cause drift of fine negative features because scattered light from pixel boundaries initiates polymerization beyond the intended voxel. The practical exposure window is therefore machine-specific and must be calibrated with a calibrated grayscale test target such as a coin or honeycomb artifact, with dimensional verification per ISO 1101.
The conversion from a printable photopolymer to a high-temperature tool is dominated by the post-cure thermal history. If the thermal stage is omitted or shortened, residual acrylate double bonds remain, and the HDT falls below the published 230 °C. Fourier-transform infrared conversion measurements alone do not replace the manufacturer’s specified time-temperature cure protocol. In applications operating at 180–220 °C, differential thermal expansion between the cured resin and metal inserts becomes significant; the polymer is expected to have a higher coefficient of thermal expansion than aluminum or steel. Published CTE data for this specific product are limited, so differential movement should be measured per ISO 11359-2 or ASTM E831 on printed test specimens. For short-run injection tools, linear shrinkage should be measured on a standardized 50 mm gauge block printed in the production orientation. Fastener bosses and sealing lands should be reinforced with metallic inserts because the resin’s tensile edge strain is limited to approximately 1–2%.
The thermal post-cure oven must provide forced-air uniformity within ±5 °C across the chamber. Large temperature overshoot above the manufacturer’s limit can generate residual stress at the interface between the UV-cured skin and thermally cured core, leading to delamination in parts with wall thickness above 10 mm. Parts should be supported on open mesh shelves rather than stacked, because contact regions limit convective heat transfer and can produce local under-cure. The heating rate and cooling rate should be controlled to prevent warpage in unsupported flat sections. The use of a vacuum oven is not required unless the manufacturer’s protocol specifies it; positive-pressure inert-gas blanketing may be considered if oxidative darkening at the surface is observed, but it does not replace the prescribed thermal profile.
Compared with general-purpose DLP photopolymers, Loctite 3D IND147 HDT230 shifts the failure mode from ductile yielding to brittle fracture. General-purpose resins often report elongation at break above 10% per ISO 527-2 and HDT values below 60 °C at 0.455 MPa. This product reports HDT 230 °C and elongation near 1–2%. The difference makes it suitable for rigid elevated-temperature inspection gauges, soldering fixtures, and composite layup tools, but unsuitable for snap-fit housings or living hinges. Compared with metal tooling, the resin can be additively formed into conformal cooling channels without machining, but its wear resistance and thermal conductivity are lower. In glass-filled polymer injection above 200 °C, the printed tool may require metallic wear inserts and conformal cooling to survive repeated cycles. Published comparative wear data against P20 mold steel or aluminum for this specific resin are limited.
Reported usage examples for this resin class include short-run mold inserts for low-pressure injection, thermoforming tools, and fixtures for soldering or adhesive cure cycles up to 230 °C for short dwells. When the process fluid is a glycol-water coolant at 130 °C, the printed material should be tested for hydrolysis and additive leaching per ASTM D543 or ISO 175; published data for this specific product under extended coolant exposure are limited. For vacuum-assisted resin transfer molding tools, the resin can be used for low-to-moderate autoclave pressure if the tool is reinforced; direct substitution for aluminum caul plates is not supported by the available mechanical data.
Before polymerization, the product contains reactive acrylate monomers and is classified as a skin sensitizer under the current safety data sheet. Handling, cleaning, and post-cure operations require nitrile gloves, protective eyewear, and local exhaust ventilation; uncured residues must not be discharged to drains. The resin should be stored in the original opaque container at 15–30 °C and kept away from UV and sunlight. Cured parts are not automatically compliant with food-contact, pharmaceutical, or implantable-device requirements; regulatory evaluations under FDA 21 CFR, EU 10/2011, or ISO 10993 are required for those applications. For electrical or electronic housings, dielectric strength and comparative tracking index should be measured per IEC 60243-1 and IEC 60112 rather than inferred from the polymer class. Regulatory status under REACH and RoHS 2011/65/EU should be verified from the current SDS and Extended SDS for the specific grade.