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Ingeo™ Biopolymer 8052D Foam Sheet Lightweight Packaging PLA

    • Название продукта: Ingeo™ Biopolymer 8052D Foam Sheet Lightweight Packaging PLA
    • Сайт Factroy: Округ Юду, Ганьчжоу, Цзянси, Китай
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    • Производитель: Ascent Petrochem Holdings Co., Limited
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    Спецификации
    Код ТН ВЭД 125127

    Как аккредитованная фабрика Ingeo ™ Biopolymer 8052D Foam Sheet Lightweight Packaging PLA, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.

    Упаковка и хранение
    Упаковка
    Доставка
    Хранение
    Применение Ingeo ™ биополимер 8052D пены листа легкой упаковки PLA

    On high-output fresh poultry and fish portioning lines, Ingeo™ Biopolymer 8052D Foam Sheet Lightweight Packaging PLA is converted into absorbent-backed trays that replace expanded polystyrene in overwrap and modified-atmosphere formats. The foam sheet is produced on a tandem single-screw extruder with a primary screw diameter of 60–90 mm and an L/D ratio of 30:1, followed by a cooling extruder of 90–120 mm diameter and a capillary slit die. Prior to extrusion, the pellets are dried at 70–80°C for 4–6 h to <250 ppm moisture because PLA hydrolyzes in the melt barrel when moisture exceeds 0.025%. In industrial practice, the cell structure is stabilized with a nucleating masterbatch added at 0.3–1.5 wt%, and carbon dioxide is injected at 1.5–3.5 wt% in the primary stage. The target sheet density is 0.08–0.16 g/cm³ measured by ISO 845, and the 10% compressive strength is verified by ISO 844 within 150–300 kPa to maintain tray rigidity under retail stacking. The conversion route is inline plug-assist thermoforming at sheet surface temperatures of 85–110°C, with mold dwell times adjusted to prevent post-forming shrinkage beyond ±1.5% after 24 h. The finished tray is sealed with flexible lidding film at 120–145°C, and heat seal strength is tested according to ASTM F88/F88M. Food-contact compliance follows EU 10/2011 with overall migration below 10 mg/dm²; for the North American market, conformity is established under an effective Food Contact Notification. The operational boundary is the protein exudate itself: under prolonged direct liquid contact in modified-atmosphere conditions, the foam cell walls at the tray base can soften if the absorbent pad becomes saturated beyond its retention capacity. The critical processing conflict is the relationship between melt strength and die pressure. The primary extruder must hold melt temperature between 170°C and 185°C; below this window the viscosity is too high for uniform gas dispersion, while above it the polylactic acid matrix loses melt extensional viscosity and the cells rupture before the sheet enters the cooling calender. Carbon dioxide is dosed through a high-pressure injection pump, and failure to hold consistent head pressure produces pre-foaming at the screw flights and a density gradient across the sheet width. Melt temperature is tracked by an infrared pyrometer across the web, and a variation greater than ±2°C across the die width causes cell-diameter variation and visible density banding.

    When Ingeo 8052D foam sheet is converted into clear produce clamshells with anti-fog food-contact surfaces

    Anti-fog behaviour in berry, grape, and cut-salad clamshells is achieved by coextruding a food-contact skin layer containing 0.5–2.0 wt% of a non-ionic surfactant masterbatch over a core foam layer. The core layer is foamed to 0.12–0.20 g/cm³, because densities below 0.10 g/cm³ produce cell diameters above 0.5 mm that scatter visible light and raise haze beyond 80% measured by ASTM D1003. The skin layer is kept near 15–25 µm after forming to limit surfactant exudation, while the overall sheet caliper is set between 0.7 mm and 1.2 mm. The sheet is thermoformed on a plug-assisted line at 90–115°C, and the mold surface is maintained at 40–60°C to balance crystallinity development against die-cutting edge cracking. The finished clamshell is sealed with a pressure-sensitive label or cold-seal adhesive to avoid thermal distortion of the vented lid. Compliance is verified under EU 10/2011 using food simulants A, B, and C, and migration of the anti-fog additive must remain below 10 mg/dm². Adhesion failures at the seal or label point are the main conversion fault: if the skin layer contains more than 2.0 wt% surfactant, the surface energy drops below the level required for cold-seal or pressure-sensitive adhesives. A corona discharge step at 42–46 mN/m wetting tension measured by ISO 8296 is used to restore adhesion, and the treatment must be applied inline less than 24 h before sealing because PLA surface oxidation decays in humid storage. The end product is a vented clamshell for chilled fresh produce, and the performance limit is condensation puddling on the lid: if the anti-fog layer is abraded during nested transport, the surface can become tacky in high-humidity cold rooms and lose the optical effect required for retail display.

    Inside insulated parcel shippers for meal kits, frozen seafood, and temperature-sensitive pharmaceuticals, 8052D sheet is cut into rectangular panels that are laminated to kraft linerboard with a water-based polyvinyl acetate adhesive. The panel assembly is die-cut to produce a foldable liner with a nominal wall caliper of 25–40 mm when multiple sheets are layered. The sheet itself is extruded at 0.04–0.08 g/cm³, placing it in the low-density regime where cell wall thickness is minimal and the thermal conductivity measured by ASTM C518 falls in the range of 0.035–0.055 W/mK. Because the glass transition of PLA is near 55–60°C, the liner is restricted to chilled or frozen payloads; exposure above 45°C in a closed vehicle can cause panel thinning and loss of the air gap that supplies the insulation value. In formulation, the foam is foamed with 4–6 wt% carbon dioxide and contains 0.3–0.8 wt% talc masterbatch to reduce cell anisotropy at high expansion ratios. The end product is tested under ISTA 7E thermal profile protocols, and the assembled shipper must hold 2–8°C for the declared transit time when configured with phase-change gel packs. The operational boundary is condensation wicking at the liner seam; if the paper facestocks are not fully bonded to the foam, moisture absorption can delaminate the panel under 85% RH. At 0.04–0.08 g/cm³, the sheet is also susceptible to cell wall thinning and edge tearing during creasing, so the liner blank is scored on a rotary cutter with a kiss-cut depth controlled to leave the lower half of the foam web intact and prevent fracture along the fold. The lamination line runs at 15–30 m/min, and adhesive coat weight is maintained at 3–6 g/m² dry; a heavier coat weight blocks foam cells and increases thermal bridging at the paper interface.

    Downstream trackRegulatory or standard referenceTest designationKey condition or limit
    Fresh protein traysEU 10/2011EN 1186 overall migrationOverall migration limit 10 mg/dm²
    Produce clamshellsEU 10/2011ASTM D1003Haze below 80% at 0.12–0.20 g/cm³
    Cold-chain linersISTA 7EASTM C518Thermal conductivity 0.035–0.055 W/mK
    Electronics cushionsIEC 61340-5-1ANSI/ESD STM11.11Surface resistivity 108–1011 ohms
    Egg cartonsEN 13432ISO 12048Reclaim cap 15–30 wt%
    Medical device traysISO 11607-1:2019ASTM F1886/F1886MNo steam autoclave; gamma or ethylene oxide only

    Electronics cushions, static decay thresholds, and the 45°C warehouse exposure boundary

    Die-cut inserts for hard disk drives, routers, and printed circuit board assemblies use 8052D foam sheet as cushioning pads between the device and a corrugated outer carton. The sheet is produced at 0.08–0.12 g/cm³ to provide repeated shock absorption across multiple drops; cushion curve testing is carried out according to ASTM D1596, and the resulting peak acceleration is recorded as a function of static stress. Electrostatic discharge control is not intrinsic to unmodified PLA, so a migratory antistatic additive or a vapour-deposited conductive skin is applied to achieve surface resistivity between 108 ohms and 1011 ohms measured by ANSI/ESD STM11.11. The additive is compounded at 0.5–1.5 wt% in the skin layer only, because higher loadings reduce thermoform edge sharpness and can create particulate contamination. Compliance is verified under RoHS Directive 2011/65/EU, REACH Article 33, and IEC 61340-5-1 for ESD-protected areas. Compression set is assessed by ISO 1856 at 45°C and 0.05 MPa static stress for 24 h. The lower use limit is set by compression creep: PLA foam under sustained static stress above 0.05 MPa at 45°C undergoes progressive thickness loss, and published data for this specific formulation is limited, so end users should commission cushion curve testing under actual warehouse heat exposure before qualifying the part. The upper use limit is impact at low humidity; static decay is slower in polyolefin-free systems, and qualification requires surface resistivity below 1×1011 ohms by ANSI/ESD STM11.11. The end product is a rigid insert with die-cut locating features, and the operational boundary is uncontrolled transit through uninsulated metal containers during summer months, where temperatures above 45°C can reduce cushion performance before the package reaches the final mile.

    What limits scrap reincorporation in egg carton production from PLA foam sheet?

    Egg cartons and fruit divider trays made from 8052D sheet are thermoformed from a low-density foam containing 0.5–1.0 wt% nucleating masterbatch and foamed to 0.06–0.10 g/cm³. The conversion line produces edge trim and rejected units that are ground, dried, and re-fed into the primary extruder. The defining process conflict is hydrolysis and molecular weight loss in regrind: each extrusion pass raises the melt flow rate measured by ISO 1133-1:2022 at 210°C/2.16 kg, and the melt strength required to hold closed-cell geometry declines. Industrial practice caps reclaim content at 15–30 wt%, depending on the moisture history of the scrap and the number of heat histories. Before reincorporation, the regrind is dried at 60–70°C to <250 ppm moisture, and the virgin/reclaim blend is gravimetrically dosed to prevent density shifts. If reclaim exceeds 30 wt%, the visible defects include cell rupture, pinholes in the carton walls, and density variation across the formed cavity. The finished egg carton must pass top-load compression according to ISO 12048, and food-contact compliance requires EU 10/2011 with overall migration below 10 mg/dm². Compostability is verified under EN 13432 when the carton is marketed as organics-collection-compatible. The operational boundary is warehouse storage above 40°C and 50% RH, where PLA can deform under vertical stacking and the hinge creases can lose their original fold memory.

    Within cleanroom tray conversion for single-use medical device packaging, the 8052D foam sheet is converted into thermoformed trays that hold syringes, catheters, or surgical kits inside a sterile barrier system. The conversion occurs in an ISO Class 8 cleanroom, and the sheet is air-ionized before die-cutting to reduce particulate shedding and static cling. The foam density is held at 0.10–0.15 g/cm³, and the forming temperature is kept below 110°C to avoid surface ablation. Compliance follows ISO 11607-1:2019 for the sterile barrier system, ISO 11137 for gamma sterilization dose audit, and ISO 11135 for ethylene oxide cycles. Sterilization compatibility is a hard boundary: PLA foam softens near 55–60°C, so steam autoclave sterilization at 121°C is not permissible; gamma or ethylene oxide processes are required, and the dose range must be confirmed because chain scission can occur above 25 kGy. The finished tray is a rigid insert inside a coated medical-grade paper or polymeric pouch, and seal integrity is tested according to ASTM F1886/F1886M. Published data for this specific configuration is limited; each medical packaging project must generate its own migration, cytotoxicity, and particulate data before regulatory clearance.

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    Более подробное введение

    Ingeo™ Biopolymer 8052D is a polylactic acid grade supplied by NatureWorks LLC for low-density foam sheet extrusion in lightweight packaging. The resin is supplied in pellet form and is formulated to increase melt tension during physical blowing agent expansion. The D-lactide content is controlled to suppress rapid crystallisation during cooling, allowing the hot sheet to remain thermoformable. Solid-state density is 1.24 g/cm³ when measured under ASTM D792-20, and the melt flow rate is specified under ISO 1133-1:2022 at 210°C and 2.16 kg; exact lot values are reported on the supplier’s certificate of analysis rather than as a single published property. Finished foam sheet densities in the 0.10–0.40 g/cm³ range are frequently targeted for clamshells, meat trays, egg cartons, and cushioning inserts. Published data for 8052D-specific density limits at very low gas loadings is limited because cell morphology depends on tandem line configuration, die pressure, and cooling roll gap.

    What Rheological and Thermal Conditions Govern 8052D Foam Stability?

    Foam extrusion of 8052D is run on tandem lines rather than single-screw lines because the resin requires a separate cooling stage to lower melt temperature before the annular or flat die. The primary extruder is typically a co-rotating twin-screw unit with an L/D ratio between 40:1 and 52:1, configured with atmospheric and vacuum venting. Desiccant drying to a moisture content below 250 ppm is mandatory; a dew point of −40°C and an inlet air temperature of 80°C for 4 h are commonly used for pellet conditioning. The melt temperature profile is set between 170°C and 200°C in the plastication zone, then reduced to 140–160°C at the die to increase elongational viscosity. Physical blowing agents, including CO₂ and N₂, are injected after the melting section; industrial starting concentrations typically fall between 0.5 wt% and 2.0 wt%, but published data for 8052D-specific gas solubility is limited. A gear pump between the primary extruder and the cooling extruder maintains die pressure within 80–150 bar to keep the blowing agent in solution and prevent pre-foaming in the melt stream.

    Melt strength is the controlling variable. In extensional rheometry, 8052D is expected to show higher strain-hardening than general-purpose PLA because its chain architecture is designed to increase entanglement density and restrict melt relaxation. Dynamic oscillatory shear at 180°C typically shows a storage-modulus crossover at a lower frequency than unmodified PLA; published data for 8052D-specific crossover frequency is limited. Capillary rheometry from 170°C to 190°C is used to fit the Carreau–Yasuda model for die pressure prediction. Extensional viscosity measurements using a Göttfert Rheotens device indicate higher melt tension than standard PLA at equivalent melt flow index; this is the primary reason for selecting 8052D in low-density foam sheet.

    Cell nucleation density depends on pressure drop rate at the die. For 8052D, the die is fitted with a low-angle converging lip and a land length selected to generate a high pressure drop rate; published data for the exact nucleation efficiency is limited. Nucleation is typically enhanced with talc or calcium carbonate at 0.1–1.0 wt%, but talc loadings above 1.5 wt% increase open-cell content and reduce melt strength because the particles act as stress concentrators in thinning cell walls. Closed-cell content above 90% is generally targeted for thermal insulation and cushioning when measured by ASTM D6226-21 gas pycnometry. A stable operation produces closed-cell foam with a mean cell diameter below 200 µm and a density reduction of at least 40% relative to solid sheet; published data for this specific configuration is limited because cell morphology depends on die geometry, gas loading, and cooling roll gap.

    Mechanical property retention in foamed 8052D follows relative-density scaling rather than simple weight reduction. For a closed-cell foam at 50% relative density, the elastic modulus typically falls to approximately one-quarter of the solid-sheet value, consistent with the Gibson–Ashby model with a quadratic dependence on relative density. The solid reference sheet commonly exhibits a tensile modulus in the 3.0–3.5 GPa range by ASTM D638-14, tensile strength in the 50–60 MPa range, and elongation at break below 10%. These values place 8052D foam in a lower toughness class than impact-modified PLA or expanded polystyrene, which constrains its use in drop-sensitive foodservice packaging unless the sheet is laminated, densified at the surface, or geometrically reinforced by ribbing.

    Compared with general-purpose PLA extrusion grades, 8052D favours lower foam density and thicker cell walls under the same blowing agent loading. Its disadvantage is a narrower moisture tolerance and more shear sensitivity at high screw speeds. Excessive specific mechanical energy input in the primary extruder can cause chain scission and reduce melt strength; converters limit screw speed and melt temperature rather than pushing throughput beyond the grade’s stable processing window. The foam sheet also requires higher preheating temperature and longer cycle time than solid PLA sheet because the insulating nature of the foam reduces heat transfer through the sheet thickness.

    Food-Contact Compliance Matrix and Migratory Boundaries

    Because 8052D is used in food-contact foam, regulatory status must be verified at the finished-article level. The base resin may be cleared for food-contact use under applicable national or regional frameworks, but the foam sheet consists of the polymer plus blowing agent residues, processing aids, and potential lactide monomer. Overall migration testing under EU Regulation No 10/2011 uses EN 1186-1:2002 and simulants selected from the regulation’s Annex III; the generic overall migration limit is 10 mg/dm² for articles intended for general food contact. For US applications, compliance is assessed under 21 CFR 174.5 and any applicable food contact notification; converters must confirm that the finished foam, including any nucleating agent or anti-static additive, meets the intended use conditions rather than assuming that the base resin certificate alone is sufficient.

    Regulatory framework or propertyRequirement or limitTest method or reference
    European Union food contactOverall migration ≤ 10 mg/dm²EU Regulation No 10/2011; EN 1186-1:2002
    United States food contactFinished-article suitability under GMP21 CFR 174.5; FDA migration guidance
    REACH SVHC content0.1 wt% per articleEC No 1907/2006
    Bio-based carbon contentTypically ≥ 95% biogenic carbonASTM D6866-21
    Industrial compostability90% disintegration after 12 weeks; ≥ 90% biodegradation after 180 daysEN 13432; ASTM D6400

    Residual lactide monomer is the primary migratory and organoleptic risk. PLA hydrolyses slowly under ambient humidity, but melt processing above 240°C accelerates chain scission and regenerates lactide, which can migrate into fatty food simulants. Converters typically specify a residual lactide target below 0.5 wt% for organoleptic neutrality; published data for 8052D-specific lactide residuals is limited, so certificate-of-analysis verification is required for each batch.

    Chemical blowing agents based on azodicarbonamide are not used in food-contact foam produced from 8052D. Physical blowing agents or food-safe endothermic nucleators are preferred because azodicarbonamide decomposition by-products are restricted under EU Regulation No 10/2011. Sodium bicarbonate–citric acid nucleating systems can be used at low loadings below 2 wt%, but they increase moisture sensitivity and require venting of water vapour. The finished foam must also meet the applicable heavy metal and ecotoxicity test batteries before an industrial compostability claim is made.

    Operational boundaries include a maximum continuous melt temperature of 230°C to avoid thermal degradation, and storage of opened pellet containers under relative humidity below 50% to prevent moisture regain. The grade should not be combined with amine-based nucleating agents or certain metal stearates that catalyse hydrolysis and reduce molecular weight during extrusion. Exposure to boiling water or retort conditions is outside the intended use window because the heat deflection temperature of amorphous PLA is below 60°C, and crystallisation in low-density foam is difficult to achieve without foam collapse.

    When 8052D Replaces Conventional Polystyrene or General-Purpose PLA Foam

    Substitution of 8052D for expanded polystyrene on an existing tandem foam line is not a drop-in change. Polystyrene foam lines usually operate with lower melt temperatures and less aggressive cooling than PLA requires; PLA melt exits the die with lower viscosity and higher stickiness on polished chrome rolls unless roll temperatures are reduced below the glass transition region. For 8052D, cooling roll temperatures are often set between 20°C and 40°C, while polystyrene lines may run warmer. Gas injection calibration must also be adjusted because CO₂ solubility and diffusivity in PLA differ from those in polystyrene; published data for this specific configuration is limited, and line trials are required to establish the stable density window.

    Compared with general-purpose PLA grades such as 2003D, 8052D has a lower melt flow index and higher melt tension. This makes it less suitable for high-speed cast film or biaxially oriented film without reformulation because the molecular architecture is biased toward melt elasticity rather than rapid draw-down. Compared with injection-moulding PLA grades such as 3052D, 8052D is not suitable for high-speed filling of thin-wall moulds. Compared with crystallised PLA sheet for hot-fill packaging, 8052D foam has lower temperature resistance and should be limited to cold-fill, short-contact warm-fill, or dry goods packaging unless post-crystallised.

    Production-line failure modes observed on tandem foam sheet equipment include pre-foaming at the die, melt fracture at the die lips, and sheet sag after the cooling rolls. These failures are corrected by raising die pressure through a melt pump, reducing gas loading, or lowering the melt temperature at the die to increase elongational viscosity. Batch-to-batch variance in melt flow rate within the supplier specification can shift the stable foam density by more than 10%; therefore, certificate-of-analysis data should be integrated into the line control system rather than using a fixed recipe across batches.

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