| Код ТН ВЭД | 855189 |
Как аккредитованный завод Lehvoss LUVOCOM 3F PAHT CF 9743 BK Nylon, Mineral Filled, для Additive Manufacturing, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.
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In low-pressure environmental control system ducting, LUVOCOM 3F PAHT CF 9743 BK is printed in segments with a 0.15 mm layer height and 100 % infill on a heated-chamber fused filament fabrication system equipped with a hardened steel nozzle of 0.4 mm diameter. The extrusion multiplier is held between 0.98 and 1.02 because over-extrusion creates lateral flash that reduces dimensional conformity of flanged coupling faces. Bed adhesion is produced on a carbon-fibre-reinforced polyimide or PEI sheet at 100–110 °C. Chamber setpoint is maintained at 60–80 °C to limit crystallisation-induced warpage in thin unsupported walls. After build, the duct segments are stress-relieved under nitrogen or recirculating air at 140 °C for 2 h, followed by natural cooling to prevent skin-core stress cracking. Terminal products include short-run cabin riser tubes, clamp collars, and environmental control system diffuser adaptors.
Airworthiness for cabin duct components is not inferred from the raw compound datasheet. Each final printed part must be tested under 14 CFR 25.853(a) Appendix F Part I or 14 CFR 25.853(d) at the minimum production thickness. Flammability, smoke density, and heat release values can shift with build orientation and filler distribution. Parts built with the tensile axis crossing layer interfaces may exhibit reduced char formation compared with XY-plane surfaces. Mechanical conformity is evaluated per ISO 527-2:2012 on conditioned specimens and ISO 75-2:2013 under 1.8 MPa flexural load. Specimens cut from curved duct walls frequently show tensile strength reductions of 20–40 % when the load axis crosses interlayer boundaries. This orientation-dependent reduction must be incorporated into the design allowable for pressurised or low-negative-pressure air handling components.
Automotive fluid-management brackets and steering knuckle prototypes are produced in short runs when machined glass-fibre-reinforced nylon 66 blanks are unavailable or lead time is excessive. The filament is dried at 100 °C for 4–6 h to a residual moisture below 0.02 wt% before loading into the extruder. Undried material generates steam splay, surface porosity, and reduced interlayer diffusion. A direct-drive extruder with a hardened steel nozzle of 0.6 mm diameter is held at 290–300 °C; the larger orifice suppresses clogging from mineral and carbon fibre agglomerates and permits a 0.2 mm layer height. Infill ratio is set at 80 % triangular grid because full-solid parts increase internal heat retention and produce curl on long flat sections. The printer chamber is kept at 70 °C and the bed at 100 °C for warpage control.
The stabiliser-to-polyamide ratio is fixed by the compound supplier. No shop-floor dilution with unfilled polyamide is permissible because lowering filler content changes shrinkage, flammability, and glycol resistance. Chemical exposure validation follows ISO 16750-5:2010 for chemical agents, with immersion in 50/50 vol% ethylene glycol/water at 120 °C for 168 h. Tensile retention after exposure is measured per ISO 527-1:2019. A retention below 80 % of unexposed strength triggers redesign, coating, or material substitution. Terminal parts include coolant pipe brackets, sensor mounting lugs, and hybrid front-end carrier inserts. Published data for this specific compound under glycol ageing is limited; each production batch must be validated because mineral filler surface chemistry can shift with supplier lot and moisture history.
Thread protectors and temporary handling fixtures for drill-pipe connections are built with a chamber temperature of 70 °C and a layer height of 0.25 mm to reduce production time for low-volume well operations. The infill ratio is 50 % with a cubic subdivision pattern, except for the threaded region which is printed with 100 % perimeters and 0.1 mm layer height to capture thread root geometry. An extrusion multiplier of 0.97 is maintained in the threaded section to prevent inter-thread binding after cooling. The printed external threads are chased with a standard pitch gauge after annealing because linear shrinkage of 0.3–0.5 % occurs along the long axis during post-crystallisation. A heated bed at 110 °C and a PEI adhesion film reduce lifting at the open ends of large protector shells.
For sour gas environments containing wet H₂S, the printed component must be assessed under ISO 23936-2:2011 or NORSOK M-710:2014 if any sealing function is expected. This compound is not a seal material. It is applied only as protective tooling and temporary handling hardware. Hardness retention and swelling are evaluated after exposure to a hydrocarbon-water test fluid at 100 °C and 24 bar for 28 days. Dimensional change exceeding 2 % in any axis disqualifies the part for field use. Terminal products include thread protectors, lifting caps, and drift mandrel storage saddles. Combined exposure to hydrogen sulphide, methanol, and monoethylene glycol at high temperature requires additional validation because the mineral filler interface can accelerate fluid ingress if surface cracks are present.
Vacuum forming tools for short-run production of amorphous thermoplastic sheet are produced with a solid shell thickness of 6 mm and 40 % gyroid infill beneath the surface to balance vacuum channel integrity and thermal mass. The tool is printed with a nozzle temperature of 285 °C and chamber setpoint of 80 °C. The build plate is a carbon-fibre-epoxy composite maintained at 110 °C. After build, the tool face is sealed with a solvent-free epoxy sealer to prevent sheet material from penetrating the printed surface. Vacuum holes are drilled, not printed, using a 0.8 mm carbide drill at 500 RPM to avoid delamination at hole edges. Terminal products are forming tools for PETG and ABS equipment covers, with surface temperature during forming not exceeding 140 °C for a cycle time of 40 s.
Dimensional stability of the tool after repeated thermal cycling is evaluated per ISO 527-2:2012 and ASTM D648-18. The forming-surface temperature limit is anchored to heat deflection temperature under 1.8 MPa. If the tool is run above 160 °C, the mineral-filled high-temperature polyamide softens and compressive creep causes vacuum hole closure. Air flow through the tool is measured with a calibrated anemometer to confirm uniformity. Deviations greater than 10 % between zones indicate plugged pores or residual powder. No direct food-contact use is claimed. Compliance for packaging tooling must be evaluated under EU 10/2011 on the finished part, not on the raw compound.
The mineral-filled high-temperature polyamide is used for reflow-compatible assembly fixtures and low-volume electronic enclosures when vapour-phase soldering processes peak at 230 °C. The build uses a 0.25 mm nozzle, 0.1 mm layer height, and 100 % infill to reduce trapped air and outgassing during thermal cycling. Drying of the filament before build is 100 °C for 6 h. After build, the enclosures are annealed in nitrogen at 180 °C for 1 h to complete crystallisation and reduce gas release during soldering. Weight loss after ageing at 230 °C for 10 min is measured by thermogravimetric analysis. A mass loss exceeding 0.15 wt% indicates incomplete drying, surface contamination, or additive degradation.
Electrostatic discharge properties are quantified per IEC 61340-5-1:2016 and surface resistivity per IEC 62631-3-2. Carbon fibre/mineral-filled polyamide grades typically exhibit conductive to static-dissipative surface resistivity, but printed surface finish and post-treatment can shift the value by orders of magnitude. The terminal parts include solder paste stencil storage trays, reflow pallet inserts, and connector positioning fixtures. The UL 94 rating for the final enclosure must be verified on the exact wall thickness produced. The presence of carbon fibre and mineral filler may produce HB rather than V-0 behaviour at 1.5 mm unless the specific grade carries a valid UL Yellow Card for that thickness and colour.
In large-format additive manufacturing, the main variable for interlayer fracture toughness is not nozzle temperature alone but the annealing sequence after build. The recommended post-build cycle begins with a 1 °C/min ramp from chamber temperature to 150 °C, a hold time of 2 h per 25 mm of maximum wall thickness, and a cooling rate no greater than 0.5 °C/min down to 80 °C. Failure to control cooling crystallises the skin faster than the core, producing residual tensile stress at layer interfaces. Property outcome is measured with Mode I interlaminar fracture toughness testing following ASTM D5528-13, with process-specific modifications because the crack path does not follow a continuous unidirectional fibre direction. Published data for this specific configuration is limited; print-orientation-specific results must be generated before structural use.
For engineering fixtures and modular jigs, the infill ratio is set at 60 % with an anisotropic infill pattern oriented 45° to the primary load axis. The extrusion multiplier is reduced to 0.96 on long linear spans to accommodate bead expansion after annealing. Build plate adhesion requires a polyimide film at 100 °C. No release agent is used because common silicone sprays migrate into the melt and reduce re-coating adhesion. Terminal products are assembly jigs, C-frame inspection fixtures, and robot gripper bases. Dimensional verification after annealing uses ISO 2768-1:1989 linear tolerances. Shrinkage corrections of 0.4 % in the build plane and 0.6 % in the Z-axis are applied at the CAD scale to compensate for anisotropic crystallisation and filler orientation.
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Lehvoss LUVOCOM 3F PAHT CF 9743 BK is a black carbon-fibre-reinforced high-temperature polyamide compound supplied in filament form for material extrusion additive manufacturing. Although category listings may describe the broader product family as “Nylon, Mineral Filled,” the “CF” designation identifies discontinuous carbon fibre as the primary reinforcing phase in this specific grade, while “BK” is the black colour identifier. The product is intended for fused filament fabrication of functional prototypes, assembly fixtures, forming tools, machining aids, and short-run production components that require higher stiffness, lower thermal expansion, and better creep resistance than unfilled or mineral-filled PAHT grades.
Specifications for this material are controlled by the current Lehvoss technical data sheet, the safety data sheet, and the published processing guide. All values cited here are indicative and should be verified against the revision issued for the production lot. Mechanical test data for printed specimens are generated according to ISO/ASTM 52921:2013 for specimen naming and build orientation and are commonly reported in XY and Z orientation under ISO 527-1:2019, ISO 527-2:2012, ISO 178:2019, and ISO 75-1:2020.
Before extrusion, the material is dried in a desiccant or vacuum dryer at 80 °C to 100 °C for 4 h to 12 h. For open-feed systems, the dew point of the drying air should be below -20 °C. The target residual moisture is below 0.05 wt% because hydrolytic chain scission of the high-temperature polyamide matrix becomes measurable above 0.10 wt% at melt temperatures. Batch-to-batch variation in moisture content is a documented failure mode when filament is left exposed to ambient relative humidity above 50 % for more than 4 h in unsealed conditions.
The extrusion temperature at the nozzle is normally set between 300 °C and 330 °C. A hardened steel, nickel-chromium, or ruby-tipped nozzle with a diameter of 0.4 mm or 0.6 mm is required; a brass orifice wears rapidly because of the discontinuous carbon fibre content, and measurable diameter drift can occur after 1 kg to 3 kg of throughput. The build platform temperature is maintained at 100 °C to 130 °C. A passively or actively heated build chamber in the range of 65 °C to 90 °C is used to limit warpage and delamination at the layer interface. Chamber temperature below 60 °C raises the risk of corner lifting and interlayer cracking in components with long continuous toolpaths or wall thicknesses above 4 mm.
Printing speed is typically set between 35 mm/s and 60 mm/s for a 0.4 mm nozzle and is adjusted to keep volumetric flow rate below approximately 8 mm³/s to 12 mm³/s. Retraction distance is kept between 0.5 mm and 1.2 mm at 20 mm/s to 30 mm/s for direct-drive extruders. The part-cooling fan is disabled or limited to 0 % to 20 % because rapid superficial cooling increases crystallisation gradients and amplifies warpage. A 0.15 mm to 0.25 mm layer height is used for the balance between interlayer bonding and deposition time.
At idling temperatures above 300 °C, the melt residence time in the hot zone should be kept below 10 min to 15 min. Prolonged idle at extrusion temperature can generate molecular weight reduction and carbon-fibre agglomeration near the nozzle constriction. After idle periods longer than 15 min, a purge length of 50 mm to 100 mm is typically discarded until a smooth, continuous extrudate with no surface voids is observed. These measures are based on production floor failure reports in which thermal degradation caused nozzle clogging and intermittent extrusion in reinforced PAHT filament.
Adhesion to unheated polyetherimide or borosilicate glass build surfaces is improved with a thin, dried polyamide-compatible adhesive film. Carbon-fibre-filled PAHT can bond so strongly to unprepared PEI that part removal damages the build sheet; a release-compatible adhesive layer or a flexible spring-steel build plate is therefore preferred for production batches. The material is not recommended for open-print environments without local exhaust ventilation because the heated ejection of reinforced filament generates particulate emissions that must be controlled under the printer operator’s workplace exposure assessment.
In direct-drive systems, filament handling is preferred over long bowden tubes because the stiff, brittle filament can buckle or fracture when fed through constrained paths with bend radii below 150 mm. In printer configurations where a bowden feed is unavoidable, a low-friction reverse-bowden guide with an inner diameter of 2.2 mm to 2.8 mm reduces drag and prevents filament scoring. These constraints are drawn from production-scale behaviour on enclosed FFF machines with build volumes up to 300 mm cube; published data for printer-specific configurations beyond that size is limited.
Material property data for FFF grades must be interpreted in terms of print orientation. The following table summarises representative property ranges for the LUVOCOM 3F PAHT family when specimens are built in the XY orientation and tested according to the indicated standards. The values are not a substitute for lot-specific certificate data but provide a comparative envelope for unfilled, glass-fibre-reinforced, and the CF 9743 BK grade.
| Property | Test method | Unfilled PAHT | PAHT GF | PAHT CF 9743 BK |
|---|---|---|---|---|
| Tensile stress at break, XY | ISO 527-1/-2 | 60–85 MPa | 80–110 MPa | 95–125 MPa |
| Tensile modulus, XY | ISO 527-1/-2 | 2.8–3.5 GPa | 5.5–7.0 GPa | 8.0–10.5 GPa |
| Flexural strength, XY | ISO 178 | 90–120 MPa | 120–160 MPa | 140–180 MPa |
| HDT B, 0.45 MPa | ISO 75-1/-2 | 100–130 °C | 160–190 °C | 190–210 °C |
| Density | ISO 1183-1 | 1.12–1.18 g/cm³ | 1.20–1.30 g/cm³ | 1.22–1.28 g/cm³ |
For the CF 9743 BK grade, the carbon fibre lowers the coefficient of linear thermal expansion in the XY plane relative to unfilled high-temperature polyamide. Published data for the exact grade-specific CLTE in the Z direction is limited; however, FFF deposition of discontinuous-fibre-filled semi-crystalline polyamide typically produces Z-direction thermal expansion closer to the matrix value because of the uninterrupted polymer-rich interlayer domain. This anisotropy must be accounted for in tolerance calculations for parts with critical hole-to-hole dimensions across multiple build layers.
Mechanical anisotropy follows the same logic. Tensile strength in the Z orientation commonly falls to 40 % to 60 % of the XY value for carbon-fibre-reinforced PAHT processed by FFF, depending on chamber temperature, layer height, and extrusion temperature. Interlayer fusion is improved by maintaining the melt temperature at the upper end of the processing window and by minimising the time between the deposition of adjacent layers. For geometrically stable tooling, a dwell time that allows the previous layer to reach a temperature near the crystallisation onset is more effective than increasing print speed.
Raster angle modifies the measured tensile modulus in the XY plane. When tensile specimens are built with all raster lines parallel to the load axis, the modulus approaches the upper end of the reported range; when the same specimens are built at ±45° or with alternating orthogonal layers, the effective tensile modulus can decrease by 20 % to 40 %. This dependency is more pronounced for the carbon-fibre-filled grade than for unfilled PAHT because the discontinuous reinforcement is aligned by the extrusion flow and does not fully randomise across layer interfaces. Mechanical testing of a representative build orientation is therefore part of first-article approval for load-bearing components under ISO 527-2.
Moisture uptake after printing reduces the glass transition temperature and tensile modulus of the polyamide matrix. Conditioning under ISO 1110 may be used to stabilise parts before dimensional inspection; dimensional changes of 0.5 % to 1.5 % can occur in uncontrolled humid environments for unfilled or lightly filled polyamides, while carbon fibre constrains volumetric expansion but does not eliminate it. For close-tolerance fixtures, parts should be annealed or conditioned in a controlled environment before final machining or metrology.
In forming tools for thermoforming or composite layup, the material is exposed to contact temperatures that may reach 130 °C to 160 °C for short cycle times. The suitability of the CF 9743 BK grade for a specific mould surface must be confirmed by thermal ageing tests under the actual contact pressure and exposure duration; published data for this specific configuration is limited, but continuous exposure above the heat deflection temperature can produce localised surface marking and reduction of flexural modulus under ISO 178. For low-contact-pressure vacuum fixtures operated below 90 °C, the material is an alternative to machined aluminium tooling when electrically conductive or non-marring surfaces are acceptable.
The carbon-fibre-filled grade is used in high-stiffness robotic end-effectors, CNC workholding jaws, inspection gauges, and pick-and-place nests. In such parts, the build orientation is set so that bending loads act along the XY plane; loading across the layer interface is avoided or reduced by increasing wall loops and using a solid infill in the load-bearing region. On production machines with a build chamber maintained above 70 °C, the interlayer tensile strength measured on printed tensile bars is less variable than on open-frame machines; the absolute value remains orientation-dependent and must be tested as part of process capability studies.
The grade should not be substituted with a generic mineral-filled nylon data sheet or with an unfilled PAHT grade. Mineral-filled polyamide products are commonly formulated to improve low-warp dimensional stability and surface finish, but their tensile modulus and heat deflection temperature are lower than those of a carbon-fibre-filled PAHT in the XY build orientation. The CF 9743 BK grade is distinguished from the mineral-filled LUVOCOM 3F PAHT variants by its higher specific stiffness, lower creep under mechanical load, and a more pronounced difference between XY and Z mechanical properties.
Compared with the glass-fibre-reinforced LUVOCOM 3F PAHT grade, the carbon-fibre-reinforced version provides higher tensile modulus and a darker, more wear-resistant surface, but it also introduces a higher risk of nozzle abrasion and may exhibit measurable surface electrical conductivity. If electrical insulation is a requirement, the glass-filled or mineral-filled grade should be evaluated under the specific voltage and frequency conditions; surface resistivity and dielectric strength should be confirmed according to IEC 62631 and IEC 60243 rather than inferred from material class.
Compared with high-temperature amorphous filaments such as polyetherimide or semicrystalline materials such as PEEK, the PAHT CF 9743 BK grade is processed at a lower extrusion temperature and can be used on a wider range of closed-chamber FFF machines. Its continuous-use temperature is lower than PEEK and its moisture absorption is higher than polyetherimide; therefore, dried storage and pre-printing moisture control are mandatory boundary conditions. The use of a mineral-filled nylon specification as a proxy for this product creates three risks: underestimation of interlayer thermal expansion, overestimation of Z-direction interlayer strength, and incorrect nozzle material selection.
Field experience on twin-screw compounding lines for carbon-fibre-filled polyamide highlights that fibre-length retention during masterbatch production and filament extrusion controls final stiffness. Fibre attrition in a co-rotating twin-screw extruder with a screw L/D ratio of 24:1 to 40:1 can reduce the final fibre length below the critical length for effective load transfer. Filament produced with excessive shear heating can show higher melt flow rate under ISO 1133-1 but lower mechanical performance; this trade-off is monitored through melt viscosity and filament diameter consistency. For the end user, filament diameter tolerance should be verified with a laser or dual-axis micrometer across the spool; outlier regions above ±0.05 mm can cause extrusion flow variation and localised porosity.
Support structures for the material are typically removed mechanically; water-soluble PVA supports are unsuitable because the high build chamber temperature and prolonged heat exposure degrade PVA at the interface. Breakaway supports printed in the same material or a dedicated PA support grade are used where overhangs exceed 45°. The use of support roofs and dense interfaces should be validated because the high melt temperature of the CF 9743 BK grade can fuse to adjacent support surfaces more strongly than unfilled PAHT.
Regulatory compliance with EU REACH and RoHS Directive 2011/65/EU should be confirmed against the current declaration issued for the specific production lot. The carbon-fibre-filled PAHT product is not intended for food-contact or medical applications unless explicitly cleared by the manufacturer.
The product is stored in sealed containers with desiccant at ambient temperatures below 30 °C and relative humidity below 20 %. Before resumed printing after storage, the filament is re-dried at 80 °C for 4 h to 6 h. Failure to re-dry after exposure to ambient humidity above 60 % is a recurring cause of steam discharge from the nozzle, which appears as surface hazing and reduced interlayer tensile strength under ISO 527-2.