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MicroFine™ Protoyping Resin

    • Название продукта: MicroFine™ Protoyping Resin
    • Сайт Factroy: Округ Юду, Ганьчжоу, Цзянси, Китай
    • Запрос цены: admin@ascent-chem.com
    • Производитель: Ascent Petrochem Holdings Co., Limited
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    Спецификации
    Код ТН ВЭД 634080

    Как аккредитованный завод MicroFine™ Prototyping Resin, мы соблюдаем строгие протоколы качества - каждая партия подвергается строгим испытаниям для обеспечения последовательных стандартов эффективности и безопасности.

    Упаковка и хранение
    Упаковка MicroFine™ Prototyping Resin is packaged in a sealed 1 kg amber plastic bottle with a child-resistant cap and hazard labels.
    Погрузка контейнера (20-футовый контейнер) MicroFine™ Prototyping Resin loaded into a 20′ FCL container, palletized, secured, and shipped in compliance with transport regulations.
    Доставка MicroFine™ Prototyping Resin is shipped in sealed, UN-rated containers, upright and cushioned. Verify hazard classification via the SDS; typically non-hazardous, but protect from heat, freezing, and moisture. Include labels, SDS, and emergency contacts. Follow DOT/IATA/IMDG rules, use absorbent packing, and always confirm current regulations before shipment.
    Хранение Store MicroFine™ Protoyping Resin in a cool, dry, well-ventilated area away from direct sunlight, heat, sparks, and open flames. Keep the container tightly closed and upright in its original packaging. Protect from freezing and moisture, and avoid contact with oxidizing agents. Maintain temperatures between 15–25°C. Keep out of reach of children. Follow local disposal regulations. Do not puncture or incinerate.
    Срок годности Shelf life is 12 months from date of manufacture when stored cool, dry, in original unopened containers, away from light.
    Применение прототипной смолы MicroFine™

    Where Does MicroFine™ Prototyping Resin Displace Traditional Wax in Investment Casting?

    In precious metal casting and dental coping production, pattern accuracy is controlled by thermal expansion behaviour and ash residue after burnout. MicroFine™ Prototyping Resin is processed at layer heights of 25–50 µm to produce positive patterns with surface roughness values that can be held below 0.4 µm Ra after optimisation, as measured by optical profilometry. Wax patterns typically soften above 55°C, while high-resolution photopolymer patterns retain dimensional stability until pyrolysis begins. Investment mixing ratios for gypsum-bonded refractory powders are maintained at 100:38 powder-to-water by weight per ISO 6871. Burnout schedules require a ramp of 2–3°C/min between 150°C and 700°C, with a hold time of 2 hours at the upper plateau to reduce carbon residue. Residual ash content must remain below 0.05 wt% because carbon-rich pockets generate casting porosities if oxidation is incomplete. The casting alloys most frequently paired with this workflow are gold-silver-copper systems and cobalt-chromium dental alloys. Flask temperatures for gold alloys are typically set between 400°C and 600°C at the moment of centrifugal casting. End products include ring blanks, crown copings, and multi-unit bridge frameworks. The primary process boundary is pattern wall thickness below 0.3 mm; unfilled acrylate photopolymers generally exhibit thermal expansion coefficients from 80 ppm/°C to 120 ppm/°C, and thin sections may generate ceramic shell microcracks during expansion. Published data specific to MicroFine™ Prototyping Resin in cobalt-chromium burnout scenarios is limited, so foundries should qualify ash behaviour on a batch-controlled basis.

    For microfluidic device prototyping, channel dimensional fidelity and surface release are controlled more by the post-cure protocol than by nominal laser spot size. MicroFine™ Prototyping Resin is used to fabricate master molds for polydimethylsiloxane replica casting because the uncured acrylate surface can inhibit platinum-catalysed addition-cure PDMS. Post-cure at 60–80°C for 30–60 minutes under 405 nm LED flood exposure reduces free-radical surface species and improves PDMS crosslinking at the interface. Channel geometries between 50 µm and 300 µm width are produced with straight sidewalls when exposure energy density is balanced against feature depth. Channel floor roughness values below 0.2 µm Ra are achievable after post-curing, as verified by stylus profilometry per ISO 4287. Silane vapour treatment with trichloro(1H,1H,2H,2H-perfluorooctyl)silane for 1–2 hours under vacuum is applied to reduce PDMS mould tear-out during demoulding. Platinum-cure silicone is mixed at a 10:1 base-to-catalyst ratio by weight, degassed at –0.09 MPa for 15 minutes, and cured at 70°C for 2 hours. End products include droplet generators, concentration gradient plates, and cell culture channels requiring optical transparency. The primary process conflict occurs below 25 µm channel width, where light scattering inside the resin increases sidewall roughness and reduces dimensional repeatability. Batch-to-batch variation in pigment package can shift the penetration depth by ±15%; this requires recalibration of exposure energy density for each incoming lot.

    Dental Surgical Guide Fabrication and ISO 10993 Cytotoxicity Boundaries

    Dental modelling and surgical guide prototypes require a split evaluation: dimensional accuracy is verified under ISO 20795-1, while biological risk is assessed under ISO 10993-5 and ISO 10993-10. MicroFine™ Prototyping Resin is printed at 50 µm layer thickness on DLP systems with 405 nm LED light engines. Green-state parts are washed in 99% isopropanol for 5–10 minutes using an ultrasonic bath at 25°C. Post-curing is performed in a nitrogen-purged chamber at 60°C for 20 minutes, followed by a second cure at 80°C for 10 minutes to reduce residual monomer. Flexural modulus of unfilled acrylate photopolymers typically ranges from 2.0 GPa to 3.5 GPa when tested to ISO 178. The printed parts are used as diagnostic casts, try-in splints, and surgical drilling templates. For surgical guide use, the resin must meet mucosal contact requirements under ISO 10993-1:2018 biological evaluation planning. Prototyping-grade resins frequently contain acrylate monomers that can irritate oral mucosa if residual monomer remains above 0.1% by weight. Extraction in isopropanol at 25°C for 10 minutes reduces the leachable monomer fraction, but this step does not replace cytotoxicity testing. Prototype surgical guides used in clinical evaluation also fall under FDA 21 CFR Part 820 quality system requirements and ISO 13485 documentation controls. The operational boundary is clear: unmodified prototyping resin should not be used for long-term intraoral devices without cytotoxicity data from the specific lot. Dimensional tolerance for model accuracy is validated against a calibrated master die using ±0.1 mm point cloud deviation. Interproximal gaps smaller than 0.2 mm may experience resin pooling during printing; such areas require post-print air blow-off and additional curing to prevent dimensional drift.

    ParameterStandardAcceptance window
    CytotoxicityISO 10993-5Grade 0 or 1
    IrritationISO 10993-10No persistent erythema or oedema
    Flexural modulusISO 1782.0–3.5 GPa
    Model accuracyOptical scan vs CAD±0.1 mm

    When MicroFine™ Prototyping Resin Is Evaluated Against Flame Retardancy Requirements in Electronics Housings

    Electronic enclosure prototyping places immediate stress on heat deflection temperature and flame resistance, neither of which is intrinsically high in unfilled acrylate photopolymers. When MicroFine™ Prototyping Resin is printed at 50 µm layer height, tensile bars tested under ASTM D638-14 typically display in-plane ultimate tensile strength in the range of 30–50 MPa, but cross-layer tensile strength can fall to 60–80% of that value. Notched Izod impact values for unfilled rigid photopolymers are commonly below 20 J/m under ASTM D256. Heat deflection temperature under 0.455 MPa load is generally within 55–75°C when measured to ASTM D648; this limits use to enclosures not exposed to internal temperatures above 50°C in continuous service. Flame resistance of unfilled acrylate resins typically achieves only UL 94 HB. Achieving UL 94 V-0 requires flame-retardant additives that are normally absent from high-resolution prototyping formulations because fillers degrade optical clarity and sidewall smoothness. Dielectric strength falls between 12 kV/mm and 16 kV/mm when tested to ASTM D149. The resin is therefore used for form, fit, and assembly validation of snap-fits, cable strain reliefs, and connector shrouds. Build orientation is selected so that snap-fit deflection loads act parallel to the print plane, not across laminate interfaces. The primary failure mode observed on production lines is root cracking at snap-fit hinges after 5–10 cycles when parts are printed vertically. Amine-containing flexibilisers must not be blended into the vat because exothermic acrylate-amine crosslinking can cause uncontrolled gelation. Printed housings should not be used as production enclosures for high-energy circuits without live-part encapsulation. Imported material entering the EU must also be checked against REACH Annex XVII restrictions and RoHS Directive 2011/65/EU if prototype assemblies are evaluated alongside production parts. Published data specific to MicroFine™ Prototyping Resin under UL 94 protocols is limited; each new batch should be assessed with a vertical burn coupon before design sign-off.

    Clear automotive lens prototypes require transmission above 88% across the visible spectrum and haze below 1.5% before surface finishing. MicroFine™ Prototyping Resin can be printed as a monolithic clear part at 30–50 µm layer heights, after which wet sanding from 400-grit to 2000-grit and acrylic clearcoat spraying are necessary to close layer lines. Light transmittance and haze are verified using ASTM D1003 with a bench spectrophotometer. The refractive index of unfilled acrylate photopolymers is approximately 1.51 at 589 nm, which is acceptable for initial optical path validation of light pipes and headlamp internal collimators. Heat deflection temperatures in the range of 55–75°C under 0.455 MPa mean that clear prototypes must be kept away from halogen lamp housings where local air temperature exceeds 80°C. UV weathering under ASTM G154 Cycle 1 typically produces yellowing index changes above 10 after 200 hours in uncoated acrylate samples, so unprotected lens prototypes are limited to short-term studio lighting tests. The end products include interior light bar lenses, park lamp test pieces, and optical sensor windows used in early-stage packaging studies. The process conflict is between surface finish and dimensional accuracy: polishing removes between 20 µm and 50 µm of material, which must be compensated by printing optical surfaces with positive stock allowance. A clearcoat system with a UV absorber package rated for automotive exterior use is mandatory if the lens is evaluated in a vehicle-level appearance audit. Published data specific to MicroFine™ Prototyping Resin under full automotive weathering specifications is limited.

    RTV silicone tooling workflows utilise high-resolution resin master patterns only after a rigorous post-cure cycle that removes surface acrylate species. MicroFine™ Prototyping Resin is used to print master patterns for room-temperature vulcanising silicone moulds because the uncured acrylate surface can inhibit platinum-cure silicone crosslinking. A two-stage post-cure at 60°C for 30 minutes followed by 80°C for 20 minutes under 405 nm LED exposure reduces the inhibition risk. Tin-cure RTV silicones are more tolerant of residual acrylate but exhibit lower tear strength than platinum-cure systems when tested under ISO 34-1. The RTV mould is typically cast as a two-part block with 10:1 base-to-catalyst ratio by weight for platinum systems, degassed at –0.09 MPa for 15 minutes, and allowed to cure for 24 hours at 25°C. Relative humidity should be kept below 50% because moisture inhibits platinum-cure silicone polymerisation. The silicone mould is then used to cast polyurethane parts with mixed viscosities below 2500 mPa·s at 25°C. End products include short-run overmoulded grips, seal prototypes, and vibration-damping grommets. The master pattern must have a minimum wall thickness of 1.0 mm because thinner sections flex during silicone pouring and produce distorted mould cavities. Surface gloss of the master pattern transfers directly to the cast polyurethane part; any scanner-visible layer lines on the master will appear on the final cast elastomer. The process boundary is chemical: acrylic photopolymer masters should be sealed with a clear acrylic lacquer before platinum-cure silicone casting if surface curing inhibition is observed. Batch-to-batch differences in resin photoinitiator concentration can change the required post-cure time by ±10 minutes; therefore, a small inhibition test coupon is recommended for each new resin lot.

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    Сертификация и соответствие требованиям
    Более подробное введение

    MicroFine™ Prototyping Resin is an acrylate-urethane hybrid photopolymer formulated for photopolymerization in 385–405 nm UV-LED and laser-galvanometer stereolithography systems with 10–50 µm layer resolution. The product is supplied in three grades: MF-100, a general-purpose amber resin; MF-200-T, a reduced-viscosity transparent variant for high-speed DLP vats; and MF-300-HDT, a high-temperature blend for investment casting patterns and short-run vacuum-forming tools. Published data for this specific formulation family is limited; all numerical values in this document are derived from internal lot-release records, third-party characterization of analogous acrylate-urethane prototyping resins, and the cited international test methods.

    Product Configurations and Exposure Parameters

    Each grade is supplied in 1 kg, 5 kg, and 20 kg HDPE containers with light-protective secondary packaging. Before use, the resin is mixed in a 25 L stainless steel vessel with an anchor stirrer operating at 30 rpm for 10 min; high-shear dispersion is not required and can entrain air that increases vat foam and surface defects. Viscosity at 25°C differentiates the grades: MF-100 is specified at 320–380 mPa·s; MF-200-T at 160–200 mPa·s; MF-300-HDT at 850–950 mPa·s when measured by ISO 3219:2003 at a shear rate of 100 s⁻¹. Density after degassing is 1.10–1.14 g/cm³ by ISO 1183-1:2019.

    For 405 nm imaging, recommended exposure energy is 18–28 mJ/cm² per 50 µm layer for MF-100, 12–20 mJ/cm² for MF-200-T, and 25–40 mJ/cm² for MF-300-HDT measured at the vat surface with a radiometer calibrated to 405 nm. Formulations for 385 nm DLP projectors require an increase of 35% in exposure time to compensate for lower initiator absorbance; this adjustment is equipment-specific and should be established using an exposure finder matrix.

    Table 1 — Indicative cured property envelope at 25°C after 30 min post-cure
    PropertyMF-100MF-200-TMF-300-HDTTest method
    Tensile strength38–44 MPa33–39 MPa50–58 MPaASTM D638-14 Type V
    Tensile modulus1.7–2.1 GPa1.5–1.9 GPa2.5–3.0 GPaASTM D638-14 Type V
    Elongation at break6–9%5–8%2–4%ASTM D638-14 Type V
    Flexural strength58–64 MPa52–60 MPa75–85 MPaISO 178:2019
    Flexural modulus1.8–2.2 GPa1.6–2.0 GPa2.6–3.1 GPaISO 178:2019
    HDT at 0.45 MPa46–50°C42–46°C88–96°CISO 75-1/-2:2020
    Notched Izod impact18–24 J/m14–18 J/m8–12 J/mASTM D256-23 Method A
    Linear shrinkage after post-cure0.9–1.3%1.0–1.4%0.6–0.9%Internal QP-07, ISO 294-4 basis

    Published data for this specific configuration is limited; the values in Table 1 represent release targets and not procurement limits. Lot-specific certificates should be requested before CNC finishing or vacuum casting.

    After post-cure in a 405 nm chamber at 20–40 mW/cm² for 30 min at 60°C, the resin reaches a conversion plateau where storage modulus at 30°C changes by less than 5% over an additional 60 min exposure. This threshold is used to define the minimum post-cure for subtractive finishing operations such as wet sanding at 400–1200 grit and high-speed milling with carbide tooling below 60°C interface temperature.

    Build orientation for MF-100 is set to 30–45° from horizontal for parts with planar cross-sections larger than 50 mm × 50 mm; this reduces the projected area per layer and lowers measured separation force from 18–22 N/cm² to 7–10 N/cm² on a 140 mm × 80 mm vat with a PDMS-coated release film. Support tip diameter for MF-100 is optimized at 0.25 mm for breakaway supports and 0.12 mm for high-resolution features; tip penetration is set to 0.2 mm to maintain attachment force without leaving surface divots larger than 80 µm after finishing.

    Green-state wet sanding is performed with water-miscible coolant at 400–1200 grit; dry sanding above 40°C surface temperature causes local curing of residual monomer and the formation of a brittle surface skin that can delaminate during subsequent painting. Machining feed rates for cured MF-300-HDT are limited to 0.15 mm/tooth with single-flute carbide end mills at 20,000 rpm; the high glass transition temperature of this grade makes it prone to chip welding when cutting depths exceed 0.5 mm without air blast cooling.

    What Limits the Green-State Post-Cure Window for MF-200-T?

    MF-200-T shows a green-state processing window of ±5°C around 22°C during support removal. At build chamber temperatures below 17°C, the uncured film modulus increases enough to tear 50 µm support tips during automated removal; at temperatures above 27°C, support tips elongate and leave residual nubs exceeding 120 µm surface deviation after trimming. The resin should therefore be equilibrated in a temperature-controlled enclosure set to 22 ± 2°C before support detachment. Residual uncured monomer at the surface is removed with two sequential baths of 99.9% isopropanol: first bath 3 min with ultrasonic agitation at 40 kHz, second bath 2 min in fresh solvent. A final rinse with tripropylene glycol monomethyl ether for 30 s reduces white haze on clear MF-200-T parts.

    Post-cure in a nitrogen-blanketed UV chamber at 20 mW/cm² and 60°C for 30 min raises the resin’s degree of conversion to approximately 85% as estimated by ATR-FTIR acrylate C=C peak reduction at 810 cm⁻¹. The estimation is equipment-dependent and should be calibrated with the specific ATR crystal. Over-post-cure beyond 60 min at 80°C induces ambering in MF-200-T and a reduction of notched Izod impact by 10–15%.

    When Ambient Humidity Exceeds 60% During Vat Replenishment

    When ambient relative humidity exceeds 60% for longer than 6 h, the resin should be conditioned under dry air with a dew point of -10°C before recirculation through a 1 µm polypropylene filter. Moisture uptake in the vat produces an increase in release force and an erratic cure depth at exposure energies below 15 mJ/cm². In production environments where open vats are refilled during summer months, an in-line filter housing with 0.5 µm nylon mesh has been installed directly after the peristaltic recirculation pump operating at 0.5 L/min. This arrangement reduces particulate agglomerates that are visible as surface pits on 50 µm build layers. Avoid adding solvent or amine-based surface modifiers to the vat; amine impurities accelerate room-temperature polymerization and shorten usable vat life to less than 24 h.

    Relative to unmodified bisphenol A epoxy acrylate resins used in high-volume stereolithography, MicroFine™ exhibits lower linear shrinkage during post-cure: 0.9–1.3% for MF-100 compared with 2.2–3.0% for a standard bisphenol A epoxy acrylate under the same internal method. The difference is attributed to the urethane segment and a lower initial acrylate equivalent weight; the specific formulation of MicroFine™ is proprietary, and published comparative data for this exact chemistry is limited. When compared with high-functionality urethane acrylate resins, MicroFine™ sacrifices some tensile modulus but provides a broader exposure range of 12–28 mJ/cm² in 385 nm DLP vats where oxygen inhibition at the vat surface reduces the cure conversion of shallow-polymerizing formulations. In accelerated aging tests at 50°C and 75% RH for 168 h, the water absorption of MF-100 was 1.2% by ISO 62:2008, which is lower than typical polyester-acrylate prototyping resins that exceed 3.0% under the same conditions.

    The use case for MF-300-HDT differs sufficiently from MF-100 and MF-200-T that direct substitution is not recommended. MF-300-HDT requires significantly higher exposure energy and shows a glass transition region above 90°C; unlike MF-100, it cannot be solvent-welded with common ketone solvents and should be post-cured in a nitrogen environment to reduce surface tack. Conversely, MF-200-T is the only grade that maintains transparency above 80% transmission at 550 nm on a 3 mm section after post-cure by ASTM D1003-21.

    For MF-200-T, total luminous transmittance on a 3 mm polished section is 86–89% by ASTM D1003-21, with haze below 3% after the two-stage solvent wash. These values are achieved only when the part is post-cured in a nitrogen-blanketed chamber; oxygen inhibition during post-cure can produce a surface haze that raises diffuse transmittance above 10%.

    Coefficient of linear thermal expansion for cured MF-300-HDT measured by ISO 11359-2:2021 between 25°C and 80°C is 62–70 µm/m·°C; this value is approximately 40% lower than MF-100 and informs tooling compensation for vacuum-forming templates where the master is digitized by structured-light scanning at 20°C.

    Photo-DSC screening on representative acrylate-urethane formulations at 405 nm and 10 mW/cm² shows a peak exotherm at 4.2 s and a conversion half-time of 1.8 s. This kinetic response supports voxel depth control of 95–110 µm at 20 mJ/cm² when exposure is calibrated against a 50 µm layer thickness. Published data for MicroFine™ specifically is limited; the values are included as an equipment-calibration reference, not as a product guarantee.

    MF-300-HDT is used for investment casting patterns requiring ash residue below 0.02% after a two-stage burnout cycle: 120°C for 30 min, followed by 650°C for 60 min. The high-temperature grade expands 2.1% during the first ramp; shell cracking is minimized by a venting gate of at least 3 mm diameter. Published data for this specific configuration is limited; foundries should validate shell thickness and dewax schedule with a test pattern before committing to batch quantities.

    For silicone vacuum-casting masters, MF-100 is sealed with a two-component epoxy surface coat to prevent platinum catalyst inhibition. Without sealing, the residual acrylate surface can reduce the Shore A hardness of a platinum-catalysed RTV silicone by 8–12 points after 24 h contact.

    Vat life in an open vat at 30% RH and 22°C is specified as 7 days for MF-100 and 5 days for MF-200-T when the resin is recirculated for 15 min every 8 h. Oxygen inhibition is not the limiting factor; gradual accumulation of partially polymerized microgel across the release film increases separation force and produces print failures that occur preferentially on the left side of the build platform when the vat is oriented with the wiper return at the left edge.

    Regulatory Documentation for MicroFine™ Resin Requires Supply Chain Disclosure

    Liquid resin is classified as a skin and eye irritant; no food-contact claims apply. The cured polymer contains no intentionally added heavy metals; compliance with RoHS 2011/65/EU Annex II restrictions can be documented through supplier declarations for the individual monomers and photoinitiators. REACH SVHC content is below the 0.1% weight threshold for articles; however, uncured liquid is a mixture and relevant safety data sheet sections should be consulted before customs classification.

    Table 2 — Compliance and safety documentation status
    FrameworkItemStatus
    REACH (EC) 1907/2006SVHC declaration, Article 33Supplier declaration available for cured article
    RoHS 2011/65/EUAnnex II restricted substancesNot intentionally added
    ASTM D638-14Tensile testingLot release, Type V specimens
    ISO 178:2019Flexural testingLot release
    ISO 75-1/-2:2020Heat deflection temperatureRelease target only
    ISO 3219:2003ViscosityLot release
    ISO 1183-1:2019DensityLot release

    Uncured resin waste is not suitable for aqueous drain disposal. Liquid waste is solidified by post-curing under UV light or by mixing with an inert filler to less than 5% liquid fraction before disposal according to local regulations. Isopropanol used for part washing is contaminated with acrylate monomers and must be collected as flammable solvent waste, not released to municipal wastewater.

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